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In the recent years diesel engine developers and manufacturers achieved a great progress in reducing the most important diesel engine pollutants, NOX and particulates. But nevertheless big efforts in diesel engine development are necessary to meet with the more stringent future emission regulations. To improve the knowledge about particle formation and emission an insight in the cylinder is necessary. By using the fast gas sampling technique samples from the cylinder were taken as a function of crank angle and analyzed regarding the soot particle size distribution and the particle mass. The particle size distribution was measured by a conventional SMPS. Under steady state conditions the influence of aromatic and oxygen content in the fuel on in-cylinder particle size distribution and particle mass inside a modern 4V-CR-DI-diesel-engine were determined. After injection and ignition, mainly small soot particles were formed which grow and in the later combustion phase coagulate.