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In this paper, a new-developed forward illumination light extinction (FILE) soot measurement technique is introduced. This technique has the capability to give two-dimensional time-resolved quantitative soot measurements. Applying the light extinction theory, the line-of-sight soot volume fraction is determined by the ratio of reflected light intensities with and without a soot cloud. The advantages of this technique include its non-intrusiveness, ease of application, requirement of only one optically accessible window, and suitability for the study of transient cycle-to-cycle variations. The application of the FILE technique for diesel combustion in a constant volume chamber demonstrates the applicability and advantages of this technique. Three stages of soot formation during diesel combustion were determined using this technique.