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A rapid compression/expansion machine (RCEM) based on a single-cylinder engine was developed to understand the fundamental phenomenon of knock during spark-ignition (SI) combustion. In order to cause auto-ignition in the end-gas mixture during the flame-propagation process, and also to visualize the processes, the original head of the engine was replaced with a specially designed combustion chamber. The effects of spark timing, compression ratio and equivalence ratio on knock intensity were systematically investigated using the RCEM with n-butane fuel. In addition, the possibility of knock control by the injection of hydrogen into the end-gas region is also discussed. The experimental results indicate that a higher compression ratio, spark-ignition timing at -10 °ATDC and a stoichiometric equivalence ratio cause heavy knock. However, the knock intensity is drastically decreased with hydrogen injection.