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Collection of diesel exhaust using the Tapered Element Oscillating Microbalance (TEOM) instrument was investigated as an alternative to the traditional method of filter weighing for particulate matter mass determination. Such an approach, if successful, would eliminate considerable manual labor involved in weighing, as well as the delay of hours or days before final results were known. To avoid known artifacts in the second-by-second mode of operation, the TEOM was used in a phase-by-phase mode and was equilibrated with air of constant temperature and humidity before each measurement. Electrically operated valves were used to automate the equilibration and measurement process. The study also included a comparison between two types of TEOM filter - an older type and a new one designed by the TEOM manufacturer for more uniform flow and less flexing. Best results were obtained with the TEOM using the new filter under no-flow conditions.

Particle size distribution and number concentration were measured in the dilute exhaust of a heavy-duty diesel engine for steady-state and transient engine operation using two different dilution systems that included a full flow CVS that was coupled to an ejector pump (CVS-EP), and a double-ejector micro-dilution tunnel (DEMDT) that was connected to engine exhaust close to turbocharger outlet. Measurements were performed using a scanning mobility particle sizer (SMPS), an electrical low pressure impactor (ELPI), and a parallel flow diffusion battery (PFDB). Fuels with sulfur content of about 385 ppm and 1 ppm were used for this work. The PFDB performed well in measuring nanoparticles in the size range below 56 nm when compared with the SMPS. This was especially valid when a distinct log-normal size distribution in the size range below 56 nm in diameter, the upper size limit of the PFDB, was present.