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The liquid fuel film on the cylinder liner is believed to be a major source of engine-out hydrocarbon emissions in SI engines, especially during cold start and warm-up period. Quantifying the liquid fuel film on the cylinder liner is essential to understand the engine-out hydrocarbon emissions formation in SI engines. In this research, two-dimensional visualization was carried out to quantify liquid fuel film on the quartz cylinder liner in an SI engine test rig. In addition, comparing visualization results with the trend of hydrocarbon emissions in this engine, the effect of cylinder wall-wetting during a simulated cold start and warmed-up condition was investigated with the engine experiment. The visualization was based on laser-induced fluorescence and total reflection. Using a quartz liner and a special lens, only the liquid fuel on the liner was visualized.