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In the present study, experiments of reactivity control compression ignition (RCCI) combustion mode is performed on a single cylinder automotive diesel engine with development ECU (electronic control unit). For achieving RCCI combustion mode, low reactivity fuel (i.e., gasoline/methanol) is injected into the intake manifold, and high reactivity fuel (i.e., diesel) is directly injected into the engine cylinder. Mass of fuel injection per cycle and their injection events are controlled using ECU. This study presents the experimental investigation on the effect of high reactivity fuel injection timings on peak pressure rise rate (PPRR) and combustion stability in RCCI engine. The combustion parameters, i.e., PPRR, indicated mean effective pressure (IMEP) and total heat release (THR) are calculated from the in-cylinder pressure measurement data. In-cylinder pressure is measured using a piezoelectric pressure transducer installed on the engine cylinder head.