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The effect of biodiesel produced from waste cooking oil (WCO) on the soot particles in a compression ignition engine was investigated and compared with conventional diesel fuel. The indicated mean effective pressure of approximately 0.65 MPa was tested under an engine speed of 1200 revolutions per minute. The fuels were injected at an injection timing of −5 crank angle degree after top dead center with injection pressures of 80 MPa. Detailed characteristics of particulate matters were analyzed in terms of transmission electron microscopy (TEM), thermogravimetric analysis (TGA) and elemental analysis. Soot aggregates were collected on TEM grid by thermophoretic sampling device installed in the exhaust pipe of the engine. High-resolution TEM images revealed that the WCO biodiesel soot was composed of smaller primary particle than diesel soot. The mean primary particle diameter was measured as 19.9 nm for WCO biodiesel and 23.7 nm for diesel, respectively.

The characteristics of soot particles in an exhaust gas for low temperature diesel combustion (LTC) compared with conventional combustion in a compression ignition engine were experimentally investigated by the elemental and thermogravimetric analysis (TGA). Morphology of soot particles was also studied by the transmission electron microscopy (TEM). From the result of the TGA, the water can be evaporated until about 150°C for both combustion regimes. The soot particles for LTC contained more volatile hydrocarbons, which can be easily evaporated from 200°C to 420°C compared with conventional diesel combustion. The soot oxidation for conventional combustion occurs up to 600°C, on the other hand the particles for LTC is oxidized below 520°C. Elemental analysis showed higher oxygen weight fraction resulted from the oxygenated hydrocarbon for the soot particles in LTC. TEM has shown primary particles to be in a diameter range of 20 to 50 nm for conventional diesel combustion.