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Accurate measurement of exhaust gas temperature in internal combustion engines is essential for a wide variety of monitoring and design purposes. Typically these measurements are made with thermocouples, which may vary in size from 0.05 mm (for fast response applications) to a few millimetres. In this work, the exhaust of a single cylinder diesel engine has been instrumented both with a fast-response probe (comprising of a 50.8 μm, 127 μm and a 254 μm thermocouple) and a standard 3 mm sheathed thermocouple in order to assess the performance of these sensors at two speed/load conditions. The experimental results show that the measured time-average exhaust temperature is dependent on the sensor size, with the smaller thermocouples indicating a lower average temperature for both speed/load conditions. Subject to operating conditions, measurement discrepancies of up to ~80 K have been observed between the different thermocouples used.