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In this study, premixed charge compression ignition (PCCI) combustion was implemented using an injector that had a narrow injection angle of 70° and a moderately early injection timing of -40° crank angle after top dead center (CA ATDC). In-cylinder pressure measurements and high-speed direct imaging of the flame were performed in an optically accessible single-cylinder diesel engine. Frequency analysis of the acquired in-cylinder pressure data was carried out to obtain the frequency range of diesel knock. Meanwhile, image segmentation and a tracking algorithm based on YCbCr color space were implemented to determine the frequency range of diesel knock from the obtained high-speed image. The results show that the frequency of diesel knock was dominated by the range from 13 kHz to 15 kHz. Still, frequency with low power existed down until 7 kHz. The frequencies of the area movement were shown to be 13 kHz and, in some cases, 8.67 kHz.