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Earlier publications have demonstrated that pad and disc properties change during storage and also during the SAE J2522 Brake Effectiveness Test Procedure. The current investigation was undertaken to find out how the properties change under milder braking conditions, using the SAE J2707 Wear Test Procedure. A copper-free formulation was selected for the investigation and tested on an inertia dynamometer using a front caliper designed for a passenger car. The pad dynamic modulus changed up or down throughout the test, depending on the test conditions. The pad dynamic modulus, the pad natural frequencies and the disc natural frequencies all decreased by the end of the test. Under high-speed, high-deceleration and high-temperature braking conditions, the pad surface region permanently expands, which results in reduced dynamic modulus and also leads to reduced pad thickness loss as compared with pad weight loss.

Earlier publications show that brake pad physical properties such as hardness, modulus and natural frequencies continue to increase at room temperature over a period of 12 months and that the changes are faster during the first 3 - 6 months. The current investigation was undertaken to see how the properties might change during testing for the pads as well as for the discs. Low-copper and copper-free formulations were tested on pickup truck and passenger car brakes. In all cases, the dynamic modulus and natural frequencies are found to decrease (not increase) after the SAE J2522 performance testing, indicating that the stiffness of the pad and that of the disc decrease faster than the mass loss due to wear. Also, the inboard pad and the outboard pad change at two different rates.

Copper-free disc pads of 9 different compositions were made using a traditional hot molding process and tested to study frictional behavior. It is found that the friction coefficient consists primarily of two parts; one part controlled by the plastic deformation of the friction surface region of the disc and pad, and the second part controlled by the total wear of the disc and pads. As the plastic deformation and the wear are non-linear with respect to the load and sliding speed, the friction coefficient becomes a non-linear function of the load and speed. Under moderate braking conditions, the plastic deformation part is more significant in determining the friction coefficient while under more severe braking conditions, the wear contribution becomes more significant. The frictional behavior of a fade cycle is explained, and the correlation between brake squeal and disc wear is confirmed.

There is anecdotal evidence that disc pad wear numbers measured in thickness loss and disc pad wear numbers measured in weight loss do not show the same wear trends after wear or performance testing. However, research papers on this topic are difficult to find. Therefore, this investigation was undertaken to study and document this behavior in detail on high-copper, low-copper and no-copper (or copper-free) NAO pads. In all cases, thickness loss measurements are found to be substantially lower than expected from the weight loss data according to the SAE J2522 test schedule. This divergence is caused by pad swelling in the pad layer adjacent to the friction contact surface during brake testing at high temperatures. In addition to formulation changes, disc pad processing conditions such as mixing time and hot molding pressure are found to affect pad swelling.

Copper-free NAO disc pads of passenger cars were investigated for a combination of prior braking conditions and moisture adsorption influencing in-stop friction and noise during low-speed stops, and in-stop-friction during moderate-speed stops. Prior braking conditions and moisture adsorption strongly influence subsequent in-stop friction behavior and noise at room temperature. The low-speed in-stop friction behavior looks totally different from that of moderate-speed stops. The low-speed in-stop friction increasingly oscillates with increasing moisture adsorption and goes down towards the end of a stop, which is accompanied by increasing low-frequency noise. The moisture content needs to be quantified/specified to obtain repeatable/reproducible brake test results as the moisture is an unintended and uncontrolled ingredient of a friction material. As the disc surface roughness increases due to prior braking conditions, the friction coefficient of low-speed stops is found to decrease.

The moisture sorption-desorption kinetics of copper-free brake pads was studied in detail. The sorption-desorption behavior is dependent on the environmental temperature and humidity. At 24 °C under 54% RH, the sorption increases rapidly for a week or so identified as the first stage of sorption, enters the second stage of negligible weight gain for a month and then the third stage of rapid sorption again. With increasing moisture sorption, the pad thickness increases through the 3 stages and the dynamic modulus also increases through the 3 stages. Friction materials lose moisture rapidly at 130°C and behave like desiccants. The sorption-desorption phenomenon significantly influences the friction coefficient -- a higher moisture content leading to lower friction coefficients. It is demonstrated that the rising friction coefficient for the half a dozen braking stops at the beginning of every brake testing in general is due to moisture desorption caused by rising pad temperatures.