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In this study, the effect of volatile fractions from engine lubricating oil on diesel particle emissions were studied experimentally. One commercial CF lubricating oil was used and distilled to subtract the different volatile fractions with boiling temperature of 220 °C, 260 °C and 300 °C, respectively. Oils derived from this distillation process were applied as the lubricating oil and following engine experiments were conducted. Diesel primary particles were sampled with a costume designed thermophoretic system. A fast response particulate spectrum equipment was employed to study the size distribution and number concentration of particles in the exhaust. Transmission electron microscopy was used to characterize the size distribution of the primary diesel particles relates to different oil volatile fractions.