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The development of a new microfluidics based carbon analyzer that is capable of generating chemicals needed in the analysis is described. The analyzer design is based on several components, an electrochemical cell, a membrane conductivity sensor, and an electrochemical water de-ionizer, which utilize porous membranes such as proton exchange membrane, gas separation membrane, and ion exchange membrane n their operation. These membrane-based microfluidic devices (MBMD) allow miniaturization of the carbon analyzer into a compact instrument which will provide high sensitivity and low power consumption. Each of the membrane-based microfluidic components was fabricated and their functioning tested over a broad range of inorganic or organic carbon content in water samples.