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This work considers the performance of a NOx control system on a diesel engine and the interaction between the NOx and particulate control devices. A commercial urea-selective catalytic reduction (SCR) catalyst (twin catalytic reactors used in series) was characterized for the impact of nitrogen dioxide (NO2) on the ammonia consumption, production of nitrous oxide (N2O) and relative selectivity of the urea-SCR catalyst for NO2 versus NO when the SCR reactors were positioned downstream of a catalyzed diesel particulate filter (DPF). The aqueous urea solution was injected into the exhaust by using a twin fluid, air-assisted atomizer. It was possible to observe the role of NO2 due to the catalyzed diesel particulate filter (DPF) upstream of the SCR catalyst. This catalyzed DPF oxidizes nitric oxide (NO) in the engine-out emissions to NO2. Further, it uses NO2 to oxidize particulate matter (PM).