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The group-hole (GH) nozzle concept that uses two closely spaced micro-orifices to substitute the conventional single orifice has the potential to facilitate better fuel atomization and evaporation, consequently attenuate the soot emission formed in direct-injection (D.I.) diesel engines. Studies of quantitative mixture properties of the transient fuel spray injected by the group-hole nozzles were conducted in a constant volume chamber via the laser absorption-scattering (LAS) technique, in comparison with conventional single-hole nozzles. Specific areas investigated involved: the non-evaporating and the evaporating ambient conditions, the free spray and the spray impinging on a flat wall conditions. The particular emphasis was on the effect of one of key parameters, the interval between orifices, of the group-hole (SH) nozzle structure.