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The effect of spray/wall interaction on diesel spray flame characteristics was investigated by applying LAS (Laser Absorption-Scattering) technique, OH* chemiluminescence and two color pyrometry in a constant volume vessel. To insure the precision of this investigation, following necessary verification experiments were carried out: (1) OH* chemiluminescence and two color pyrometry were synchronously employed to analyze the influence of soot incandescence on OH* chemiluminescence signal intensity; and (2) frontal view and side view OH* images of a linearly arranged three holes injector were concentrated on to investigate the effect of soot on optical intensity attenuation under line-of-sight image recording condition. And then the effect of impinging distance (30,40,50,60 mm and free) on diesel spray and combustion behaviors were studied. The results reveal that the impinging distance plays a significant role in mixture formation.