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Exhaust emissions and combustion characteristics from well-characterized diesel test fuels have been measured using two types of single-cylinder HSDI diesel engines. Data were collected at several fixed speed/load conditions representative of typical light-duty operating conditions and full-load performance (smoke-limited maximum torque) points. In addition, in-cylinder soot formation processes of these fuels were investigated via Laser Induced Incandescence (LII) using an optically accessible single-cylinder engine. The test fuels used in this study have been formulated with a sophisticated blending algorithm that systematically varies the hydrocarbon molecular structure in the fuels while maintaining the distillation characteristics of market diesel fuels. The following results have been obtained from this study. (1) The lowest PM emissions were observed with a fuel containing approximately 55% iso-paraffins and 39% n-paraffins with CN=52.5.