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Patent-pending Metabolic heat regenerated Temperature Swing Adsorption (MTSA) technology is currently being investigated for removal and rejection of carbon dioxide (CO2) and heat from a Portable Life Support System (PLSS) to a Martian environment. The metabolically-produced CO2 present in the ventilation loop gas is collected using a CO2 selective adsorbent that has been cooled via a heat exchanger to near CO2 sublimation temperatures (∼195 K) with liquid CO2 (LCO2) obtained from Martian resources. Once the adsorbent is fully loaded, used, warm (∼300 K), moist ventilation loop gas is used to heat the adsorbent via another heat exchanger to reject the collected CO2 to the Martian ambient. Two beds are used to achieve continuous CO2 removal by cycling between the cold and warm conditions for adsorbent loading and regeneration, respectively.