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A novel diagnostic technique named a “Tracer-Producing LIF technique” which enables 2-dimensional measurement of an internal EGR within an engine cylinder, has been developed. The main feature of this technique is the utilization of a fuel additive that does not itself emit an LIF signal by irradiation of UV-light but whose combustion products radiate strong LIF emissions by UV-light irradiation. Internal EGR behaviors can be measured by observing LIF images that are excited by a UV-laser sheet. Firstly, principles of this technique were confirmed and fuel additives were selected. Then, the “Tracer-Producing LIF technique” was applied to an optically accessible single-cylinder gasoline engine in which the entire pent-roof area can be observed from the side of the engine. The internal EGR behaviors were measured through the entire engine cycle, from intake to exhaust.