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A protocol has been developed that produced the type of lunar soil abrasion damage observed on Apollo spacesuits. This protocol was then applied to four materials (Kevlar®, Vectran®, Orthofabric, and Tyvek®) that are candidates for advanced spacesuits. Three of the four new candidate fabrics (all but Vectran®) were effective at keeping the dust from penetrating to layers beneath. In the cases of Kevlar® and Orthofabric this was accomplished by the addition of a silicone layer. In the case of Tyvek®, the paper structure was dense enough to block dust transport. The least abrasive damage was suffered by the Tyvek®. This was thought to be due in large part to its non-woven paper structure. The woven structures were all abraded where the top of the weave was struck by the abrasive. Of these, the Orthofabric suffered the least wear, with both Vectran® and Kevlar® suffering considerably more extensive filament breakage.

The International Space Station (ISS) is a complex spacecraft that will take several years to assemble in orbit. During many of the assembly and maintenance procedures, the space station’s large solar arrays must be locked, which can significantly reduce power generation. To date, power generation analyses have not included power generation from the backside of the solar cells in a desire to produce a conservative analysis. This paper describes the testing of ISS solar cell backside power generation, analytical modeling, and analysis results on an ISS assembly mission.

NASA Glenn Research Center and the Wallops Flight Facility jointly conducted a PEM fuel cell power system development effort for high altitude balloon applications. This was the first phase of NASA efforts to offer higher balloon payload power levels with extended duration mission capabilities for atmospheric science missions. At present, lead-acid batteries typically supply about 100 watts of power to the balloon payload for approximately 8 hours duration. The H2-O2 PEM fuel cell demonstration system developed for this effort can supply at least 200 watts for 48 hours duration. The system was designed and fabricated, then tested in ambient ground environments as well as in a thermal vacuum chamber to simulate operation at 75 kft. altitude. Initially, this program was planned to culminate with a demonstration flight test but no flight has been scheduled, thus far.

Operational issues encountered by Apollo astronauts relating to lunar dust were catalogued, including material abrasion that resulted in scratches and wear on spacesuit components, ultimately impacting visibility, joint mobility and pressure retention. Standard methods are being developed to measure abrasive wear on candidate construction materials to be used for spacesuits, spacecraft, and robotics. Calibration tests were conducted using a standard diamond stylus scratch tip on the common spacecraft structure aluminum, Al 6061-T6. Custom tips were fabricated from terrestrial counterparts of lunar minerals for scratching Al 6061-T6 and comparing to standard diamond scratches. Considerations are offered for how to apply standards when selecting materials and developing dust mitigation strategies for lunar architecture elements.

This paper will discuss the status of the Compact Flash Evaporator System (CFES) development at NASA Glenn. Three alternative heat sink technologies are being developed under Thermal Control for Advanced Capabilities within the Exploration Technology Development Program. One of them is CFES, a spray cooling concept related to the current Space Shuttle Orbiter Flash Evaporator System (FES). In the CFES concept, water is sprayed on the outside of a flat plate heat exchanger, through which flows the vehicle's primary vehicle heat transfer fluid. The steam is then exhausted to space in an open-loop system. Design, fabrication and testing of the CFES at NASA's Glenn Research Center will be reported.

Tests designed to quantify the gravitational effects on thermal mixing and reactant injection in a Supercritical Water Oxidation (SCWO) reactor have recently been performed in the Zero Gravity Facility (ZGF) at NASA's Glenn Research Center. An artificial waste stream, comprising aqueous mixtures of methanol, was pressurized to approximately 250 atm and then heated to 450°C. After uniform temperatures in the reactor were verified, a controlled injection of air was initiated through a specially designed injector to simulate diffusion limited reactions typical in most continuous flow reactors. Results from a thermal mapping of the reaction zone in both 1-g and 0-g environments are compared. Additionally, results of a numerical model of the test configuration are presented to illustrate first order effects on reactant mixing and thermal transport in the absence of gravity.

Special coatings are being developed and tested to contend with the effects of dust on the lunar surface. These coatings will have wide applicability ranging from prevention of dust buildup on solar arrays and radiator surfaces to protection of EVA space suit fabrics and visors. They will be required to be durable and functional based on application. We have started preparing abrasion-resistant transparent conductive coatings ∼40 nm thick were formed by co-deposition of titanium dioxide (TiO2) and titanium (Ti) on room-temperature glass and polycarbonate substrates using two RF magnetron sputtering sources. By adjusting Ti content, we obtained sheet resistivities in the range 104-1010 ohms/square. We have also started conducting a series of environmental tests that simulate the exposure of coated samples to dust under relevant conditions, beginning with abrasion tests using regolith simulant materials.

The Vapor Phase Catalytic Ammonia Removal (VPCAR) system is being developed to recycle water for future NASA Exploration Missions. Testing was recently conducted on NASA's C-9B Reduced Gravity Aircraft to determine the microgravity performance of a key component of the VPCAR water recovery system. Six flights were conducted to evaluate the fluid dynamics of the Wiped-Film Rotating Disk (WFRD) distillation component of the VPCAR system in microgravity, focusing on the water delivery method. The experiments utilized a simplified system to study the process of forming a thin film on a disk similar to that in the evaporator section of VPCAR. Fluid issues are present with the current configuration, and the initial alternative configurations were only partial successful in microgravity operation. The underlying causes of these issues are understood, and new alternatives are being designed to rectify the problems.

Supercritical water oxidation (SCWO) may become an attractive technology for processing solid and liquid wastes for long duration space and extraterrestrial planetary missions. Gravitational influences on the operation of SCWO reactors are discussed in the context of key dimensionless parameters for two general modes of operation: a “premixed” mode, where the reactants are brought to supercritical temperatures and pressures simultaneously, and a “diffusion limited” mode, where one of the reactants (typically the oxidizer) is injected into the reactor after the bulk fluid is raised to supercritical temperatures and pressures. An experimental facility for testing the gravitational influences on a SCWO reactor is then discussed.

Packed bed reactors are well known for their vast and diverse applications in the chemical industry; from gas absorption, to stripping, to catalytic conversion. Use of this type of reactor in terrestrial applications has been rather extensive because of their simplicity and relative ease of operation. Developing similar reactors for use in microgravity is critical to many space-based advanced life support systems. However, the hydrodynamics of two-phase flow packed bed reactors in this new environment and the effects of one physicochemical process on another has not been adequately assessed. Surface tension or capillary forces play a much greater role which results in a shifting in flow regime transitions and pressure drop. Results from low gravity experiments related to flow regimes and two-phase pressure drop models are presented in this paper along with a description of plans for a flight experiment on the International Space Station (ISS).

An experiment was conducted in the Icing Research Tunnel (IRT) at NASA Glenn Research Center to obtain castings of ice accretions formed on a 28° swept GLC-305 airfoil that is representative of a modern business aircraft wing. Because of the complexity of the casting process, the airfoil was designed with three removable leading edges covering the whole span. Ice accretions were obtained at six icing conditions. After the ice was accreted, the leading edges were detached from the airfoil and moved to a cold room. Molds of the ice accretions were obtained, and from them, urethane castings were fabricated. This experiment is the icing test of a two-part experiment to study the aerodynamic effects of ice accretions.

A process of using machine learning to segment impact ice microstructure is presented and analyzed. The microstructure of impact ice has been shown to correlate with the adhesion strength of ice. Machine vision techniques are explored as a method of decreasing analysis time. The segmentation was conducted with the goal of obtaining average grain size estimations. The model was trained on a set of micrographs of impact ice grown at NASA Glenn’s Icing Research Tunnel. The model leveraged a model pre-trained on a large set of micrographs of various materials as a starting point. Post-processing of the segmented images was done to connect broken boundaries. An automatic method of determining grain size following an ASTM standard was implemented. Segmentation results using different training sets as well as different encoder and decoder pairs are presented. Calculated sizes are compared to manual grain size measurement methods.

Using a new fiber electrode technology, currently developed and produced by Bekaert Corporation (Bekaert), Electro Energy, Inc., (EEI) Mobile Energy Products Group (formerly, Eagle-Picher Technologies, LLC, Power Systems Department) in Colorado Springs, CO has demonstrated that it is feasible to manufacture flight weight nickel hydrogen cells having about twice the specific energy (80 vs. 40 watt-hr./kg) as state-of-the-art nickel hydrogen cells that are currently flown on geosynchronous communications satellites. Although lithium-ion battery technology has made large in-roads to replace the nickel alkaline technology (nickel-cadmium, nickel-metal hydride), the technology offered here competes with lithium-ion weight and offers alternatives not present in the lithium-ion chemistry such as: ability to undergo a continuous overcharge, reversal on discharge, and sustain rate capability sufficient to start automotive and aircraft engines at subzero temperatures.

The International Space Station Carbon Dioxide Removal Assembly (CDRA) uses regenerable adsorption technology to remove carbon dioxide (CO2) from cabin air. CO2 product water vapor measurements from a CDRA test bed unit at the NASA Marshall Space Flight Center were made using a tunable infrared diode laser differential absorption spectrometer (TILDAS) provided by NASA Glenn Research Center. The TILDAS instrument exceeded all the test specifications, including sensitivity, dynamic range, time response, and unattended operation. During the CO2 desorption phase, water vapor concentrations as low as 5 ppmv were observed near the peak of CO2 evolution, rising to levels of ∼40 ppmv at the end of a cycle. Periods of high water concentration (>100 ppmv) were detected and shown to be caused by an experimental artifact.

The on-demand production of Medical Grade Water (MGW) is a critical biomedical requirement for future long-duration exploration missions. Potentially, large volumes of MGW may be needed to treat burn victims, with lesser amounts required to reconstitute pharmacological agents for medical preparations and biological experiments, and to formulate parenteral fluids during medical treatment. Storage of MGW is an untenable means to meet this requirement, as are nominal MGW production methods, which use a complex set of processes to remove chemical contaminants, inactivate all microorganisms, and eliminate endotoxins, a toxin originating from gram-negative bacteria cell walls. An innovative microgravity compatible alternative, using a microwave-based MGW generator, is described in this paper. The MGW generator efficiently couples microwaves to a single-phase flowing stream, resulting in super-autoclave temperatures.

Manufacturing readiness of composite rotors and certification of flywheels depend in part on the maturity of nondestructive evaluation (NDE) technology for process optimization and quality assurance, respectively. Capabilities and limitations of x-ray-computed tomography and radiography, as well as advanced ultrasonics were established on NDE ring and rotor standards with EDM notches and drilled holes. Also, intentionally seeded delamination, tow break, and insert of bagging material were introduced in hydroburst-rings to study the NDE detection capabilities of such anomalies and their effect on the damage tolerance and safe life margins of subscale rings and rotors. Examples of possible occurring flaws or anomalies in composite rings as detected by NDE and validated by destructive metallography are shown. The general NDE approach to ensure quality of composite rotors and to help in the certification of flywheels is briefly outlined.

An experiment was conducted in the Icing Research Tunnel (IRT) at NASA Glenn Research Center to study the effect of sweep angle and temperature on the formation of ice accretions on a NACA 0012 swept wing at SLD conditions. From a baseline Appendix-C condition with a MVD of 20m the drop size was changed to 110 and 200m for the SLD cases. Casting data, ice shape tracings, time-sequence and photographic data were obtained. Time-sequence photography was taken during each run to capture in real time the formation of the ice accretion. Measurements of the critical distance were obtained.

Development of a high specific energy battery is one of the objectives of the lightweight nickel-hydrogen (Ni-H2) program at the NASA Glenn Research Center. The approach has been to improve the nickel electrode by continuing combined in-house and contract efforts to develop a lighter weight electrode for the nickel-hydrogen cell. Small fiber diameter nickel plaques are used as conductive supports for the nickel hydroxide active material. These plaques are commercial products and have an advantage of increased surface area available for the deposition of active material. Initial tests include activation and capacity measurements at five different discharge levels, C/2, 1.0C, 1.37C, 2.0C, and 2.74C. The electrodes are life cycle tested using a half-cell configuration at 40 and 80% depths-of-discharge (DOD) in a low-Earth-orbit regime. The electrodes that pass the initial tests are life cycle-tested in a boilerplate nickel-hydrogen cell before flightweight designs are built and tested.

This paper presents results from a smoke detection experiment entitled Smoke Aerosol Measurement Experiment (SAME) which was conducted in the Microgravity Science Glovebox on the International Space Station (ISS) during Expedition 15. Five different materials representative of those found in spacecraft were pyrolyzed at temperatures below the ignition point with conditions controlled to provide repeatable sample surface temperatures and air flow conditions. The sample materials were Teflon®, Kapton®, cellulose, silicone rubber and dibutylphthalate. The transport time from the smoke source to the detector was simulated by holding the smoke in an aging chamber for times ranging from 10 to1800 seconds. Smoke particle samples were collected on Transmission Electron Microscope (TEM) grids for post-flight analysis.

The Icing Research Tunnel at NASA Glenn follows the recommended practice for calibration outlined in SAE’s ARP5905. The calibration team has followed the schedule of a full calibration every five years with a check calibration done every six months following. The liquid water content of the IRT has maintained stability within the stated specifications of variation within +/- 10% of the curve fit equation generated from calibration data. Using past measurements and data trends, IRT characterization engineers wanted to develop methods for the ability to know when data were not within variation. Trends can be observed in the liquid water content measurement process by constructing statistical process control charts. This paper describes data processing procedures for the Multi-Element Sensor in the IRT, including collision efficiency corrections, canonical correlation analysis, process for rejection of data, and construction of control charts.