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Thermal characterization was performed on a vapor compression heat pump using a novel, hybrid two phase loop design. Previous work on this technology has demonstrated its ability to provide passive phase separation and flow control based on capillary action. This provides high quality vapor to the compressor without relying on gravity-based phase separation or other active devices. This paper describes the subsequent work done to characterize evaporator performance under various startup scenarios, tilt angles, and heat loads. The use of a thermal expansion valve as a method to regulate operation was investigated. The effect of past history of use on startup behavior was also studied. Testing under various tilt angles showed evaporator performance to be affected by both adverse and favorable tilts for the given compressor. And depending on the distribution of liquid in the system upon startup, markedly different performance can result for the same system settings and heat loads.

The Moon Mineralogy Mapper (M3) instrument is scheduled for launch in 2008 onboard the Indian Chandrayaan-1 spacecraft. The mission is managed by the Indian Space Research Organization (ISRO) in Bangalore, India and is India's first flight to the Moon. M3 is being developed for NASA by the Jet Propulsion Laboratory under the Discovery Program Office managed by Marshall Space Flight Center. M3 is a state-of-the-art instrument designed to fulfill science and exploratory objectives. Its primary science objective is to characterize and map the lunar surface composition to better understand its geologic evolution. M3's primary exploration goal is to assess and map the Moon mineral resources at high spatial resolution to support future targeted missions. M3 is a cryogenic near infrared imaging spectrometer with spectral coverage of 0.4 to 3.0 μm at 10 nm resolution with high signal to noise ratio, spatial and spectral uniformity.

NASA's Exploration Mission program is planning for a return to the Moon in 2020. The Exploration Systems Mission Directorate (ESMD)'s Lunar Architecture Team (LAT) is currently refining their lunar habitat architectures. The Advanced Thermal Control Project at the Johnson Space Center, as part of the Exploration Technology Development Program (ETDP) is developing technologies in support of the future lunar missions. In support of this project, a trade study was conducted at the Jet Propulsion Laboratory on the mechanically pumped two-phase and single-phase thermal loops for lunar habitats located at the South Pole for the LAT II architecture. This paper discusses the various trades and the results for a representative architecture which shares a common external loop for the single and two-phase system cases.

An array-based sensing system based on polymer-carbon composite conductometric sensors is under development at JPL for use as an environmental monitor in the International Space Station. Sulfur dioxide has been added to the analyte set for this phase of development. Using molecular modeling techniques, the interaction energy between SO2 and polymer functional groups has been calculated, and polymers selected as potential SO2 sensors. Experiment has validated the model and two selected polymers have been shown to be promising materials for SO2 detection.

The overall goal of this program was the development of a 10 m. diameter, self-deployable antenna based on an open-celled rigid polyurethane foam system. Advantages of such a system relative to current inflatable or self-deploying systems include high volumetric efficiency of packing, high restoring force, low (or no) outgassing, low thermal conductivity, high dynamic damping, mechanical isotropy, infinite shelf life, and easy fabrication with methods amenable to construction of large structures (i.e., spraying). As part of a NASA Phase II SBIR, Adherent Technologies and its research partners, Temeku Technologies, and NASA JPL/Caltech, conducted activities in foam formulation, interdisciplinary analysis, and RF testing to assess the viability of using open cell polyurethane foams for self-deploying antenna applications.

An array-based sensing system based on 32 polymer/carbon composite conductometric sensors is under development at JPL. Until the present phase of development, the analyte set has focused on organic compounds (common solvents) and a few selected inorganic compounds, notably ammonia and hydrazine. The present phase of JPL ENose development has added two inorganics to the analyte set: mercury and sulfur dioxide. Through models of sensor-analyte response developed under this program coupled with a literature survey, approaches to including these analytes in the ENose target set have been determined.

Certain Eubacteria enter a viable but nonculturable (VBNC) state upon encountering unfavorable environmental conditions. VBNC cells do not divide on conventional media yet remain viable and in some cases retain virulence. Here, we describe the VBNC state of two opportunistic pathogens previously isolated from ISS potable waters, Burkholderia cepacia and Stenotrophomonas maltophilia. Artificially inoculated microcosms were exposed to the biocidal agents copper (CuSO4) and iodine (I2) in an attempt to induce nonculturablility. Viability was assessed via fluorescent microscopy (direct viable count assay coupled with BacLight™ staining) and metabolic activity was monitored by quantifying both intracellular ATP and transcribed rRNA (reverse transcriptase quantitative PCR). Culturablility was lost in both B. cepacia and S. maltophilia within two days of exposure to copper or high concentrations of iodine (6 or 8 ppm).

The Mars Exploration Rover (MER) flight system uses mechanical, paraffin-actuated heat switches as part of its secondary battery thermal control system. This paper describes the design, flight qualification, and performance of the heat switch. Although based on previous designs by Starsys Research Corporation1,2, the MER mission requirements have necessitated new design features and an extensive qualification program. The design utilizes the work created by the expansion of a paraffin wax by bringing into contact two aluminum surfaces, thereby forming a heat conduction path. As the paraffin freezes and contracts, compression springs separate the surfaces to remove the conduction path. The flight qualification program involved extensive thermal performance, structural, and life testing.

A technology demonstration propylene Loop Heat Pipe (LHP) has been tested extensively in support of the implementation of this two-phase thermal control technology on NASA’s Earth Observing System (EOS) Tropospheric Emission Spectrometer (TES) instrument. This cryogenic instrument is being developed at the Jet Propulsion Laboratory (JPL) for NASA. This paper reports on the transient characterization testing results showing low frequency temperature oscillations. Steady state performance and model correlation results can be found elsewhere. Results for transient startup and shutdown are also reported elsewhere. In space applications, when LHPs are used for thermal control, the power dissipation components are typically of large mass and may operate over a wide range of power dissipations; there is a concern that the LHP evaporator may see temperature oscillations at low powers and over some temperature range.

As a result of the Viking missions in 1970s, the presence of a strong oxidant in Martian soil was suggested. Here we present a testable, by near-term missions, hypothesis that iron(VI) contributes to that oxidizing pool. Ferrate(VI) salts were studied for their spectral and oxidative properties and biological activities. Ferrate(VI) has distinctive spectroscopic features making it available for detection by remote sensing reflectance spectra and contact measurements via Mössbauer spectroscopy. The relevant miniaturized instrumentation has been developed or is underway, while XANES spectroscopy is shown to be a method of choice for the returned samples. Ferrate(VI) is capable of splitting water to yield oxygen, and oxidizing organic carbon to CO2. Organic oxidation was strongly abated after pre-heating ferrate, similar to the observations with Mars soil samples.

The development of tunable diode laser systems in the 2 - 5 μm spectral region will have numerous applications for trace gas detection. To date, the development of such systems has been hampered by the difficulties of epitaxial growth, and device processing in the case of the Sb-based materials system. One of the compounding factors in this materials system is the use of aluminum containing compounds in the laser diode cladding layers. This makes the regrowth steps used in traditional lasers very difficult. As an alternative approach we are developing laterally coupled antimonide based lasers structures that do not require the regrowth steps. In this paper, the materials growth, device processing and development of the necessary drive electronics for an antimony based tunable diode laser system are discussed.

A flight experiment to test the operation of an Electronic Nose developed and built at JPL and Caltech was done aboard STS-95 in October-November, 1998. This ENose uses conductometric sensors made of insulating polymer-carbon composite films; it has a volume of 1.7 liters, weighs 1.4 kg including the operating computer and operates on 1.5 W average power. In the flight experiment, the ENose was operated continuously for 6 days and recorded the sensors' response to changes in air in the mid-deck of the orbiter. The ENose had been trained to identify and quantify ten common contaminants at the 24-hour Spacecraft Maximum Allowable Concentration (SMAC) level. Most SMACs are on the order of 10-100 ppm. The experiment was controlled by collecting air samples daily and analyzing them using standard analytical techniques after the flight. The device is microgravity insensitive.

The Jet Propulsion Laboratory Mars Exploration Program Office is currently planning a series of exciting missions to the Red Planet. During each launch opportunity, the missions to Mars will include a Rover mission. During the earlier Rover missions to Mars such as the Mars Pathfinder mission carrying the Sojourner Rover in 1997, the main rover power source was a solar array. The power subsystem of the Sojourner Rover included a solar panel for power during the day, a non-rechargeable lithium battery for power during the night, and a power electronics board for power conditioning and distribution. Starting with the year 2003 the rover missions to Mars will incorporate a rechargeable energy storage device rather than a non-rechargeable power source. Included in the power electronics board, will be a battery controller/charger. The battery controller/charger will be able to monitor and control three parallel 4-cell battery strings.

The power produced by an AMTEC is dependent on the porosity of the electrode layers deposited on the surface of the BASE tubes. The elevated temperatures at which these power generators operate result in a slow growth or coalescence of the grains that comprise the electrode layers thereby reducing porosity and effective surface area. The lifetime of AMTEC electrodes is therefore related to the rate of grain growth of the electrode material. A preliminary model has been developed to determine the rate of grain growth over the operational lifetime of an AMTEC. This model examines the conditions for continuous growth as a function of the relative sizes, boundary and activation energies and mobilities of the grains. An assumption of strain-free growth has been made in determining the factors for normal growth. Experimental measurements for titanium nitride alloy electrodes are compared with this model. Predictions are made for performance lifetimes out to 10 years.

The lifetime of an AMTEC electrode is predicted from the rate of grain growth in the electrode. The rate of growth depends on several physical characteristics of each material, including the rate of diffusion of the material on itself. Grain growth rates for rhodium-tungsten and titanium nitride electrodes have been determined, and have been used to predict operating lifetimes of AMTEC electrodes. For lifetimes of 10 years or more, RhxW electrodes may be used at any operating temperature supportable by the electrolyte. TiN electrodes may be used in AMTEC cells only at operating temperatures under 1150 K.

This paper reports several slow reversible and quasi-reversible processes which occur in the porous electrode/solid electrolyte combination at AMTEC operating temperatures. These processes help to elucidate the evolution of the electrode and electrolyte characteristics with time. They also demonstrate that the atomic constituents of the electrode/electrolyte engage in significant dynamic motion. We report the stability of the sodium beta“-alumina phase in low pressure sodium vapor at 1173K up to 3000 hours, and the decomposition of the sodium meta-aluminate (NaAlO2) phase present at about 1% in the BASE ceramic, which gives rise to transient local increases in the solid electrolyte resistivity due to local micro-cracking. We also report slow apparent morphological changes, possibly surface or grain boundary reconstruction, in TiN and RhW electrodes driven by changes in the local sodium activity.