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Spark discharge properties were studied and characterized for varying gas compositions and spark plug geometries using a spark calorimeter and constant volume optical vessel. Two different 18 mm natural gas engine spark plugs were used in the experiments. All measurements were recorded under quiescent conditions and with a spark gap of 0.30 mm. The spark plug calorimeter was used for measuring thermal energy deposition to the gas for gas compositions of nitrogen, a stoichiometric mixture of nitrogen and methane, a stoichiometric mixture of nitrogen and methane diluted with 30% carbon dioxide by volume, and for air. Other measurements of interest included breakdown voltage, electrical energy delivered to the spark gap, electrical-to-thermal energy conversion efficiency, and spark duration, for pressures up to 28 bar at 300 K. The optical vessel was used for the combusting mixture of stoichiometric air and methane at pressures up to 28 bar.