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An experimental study was performed, using cycle-resolved laser Doppler velocimetry (LDV) technique, to characterize the exhaust flow structure inside a catalytic converter retro-fitted to a firing four-cylinder gasoline engine over different operating conditions. A small fraction of titanium (IV) isopropoxide was dissolved in gasoline to generate titanium dioxide during combustion as seeding particles for LDV measurements. It was found that in the front plane of the catalytic monolith, the velocity is highly fluctuating due to the pulsating nature of the engine exhaust flow, which strongly depends on the engine operating conditions. Under unloaded condition, four pairs of major peaks are clearly observed in the time history of the velocity, which correspond to the main exhaust events of each individual cylinder.