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This project’s objective was to generate experimental data to evaluate the impact of metals doped B20 on diesel particle filter (DPF) ash loading and performance compared to that of conventional petrodiesel. The effect of metals doped B20 vs. conventional diesel on a DPF was quantified in a laboratory controlled accelerated ash loading study. The ash loading was conducted on two DPFs – one using ULSD fuel and the other on B20 containing metals dopants equivalent to 4 ppm B100 total metals. Engine oil consumption and B20 metals levels were accelerated by a factor of 5, with DPFs loaded to 30 g/L of ash. Details of the ash loading experiment and on-engine DPF performance evaluations are presented in the companion paper (Part I). The DPFs were cleaned, and ash samples were taken from the cleaned material. X-ray Fluorescence (XRF), X-Ray Photoelectron Spectroscopy (XPS) and X-Ray Diffraction (XRD) were conducted on the ash samples.

The project objective was to generate experimental data to evaluate the impact of metals doped B20 on DPF ash loading and performance compared to that of conventional petrodiesel. Accelerated ash loading was conducted on two DPFs – one exposed to regular diesel fuel and the other to B20 containing metal dopants equivalent to 4 ppm B100 total metals (currently total metals are limited to 10 ppm in ASTM D6751, the standard for B100). Periodic performance evaluations were conducted on the DPFs at 10 g/L ash loading intervals. After the evaluations at 30 g/L, the DPF was cleaned with a commercial DPF cleaning machine and another round of DPF evaluations were conducted. A comparison of the effect of ash loading with the two fuels and DPF cleaning is presented. The metals doped B20 fuel resulted in ash that was similar to that deposited when exposed to ULSD (lube oil ash) and exhibited similar ash cleaning removal efficiency.

The engine power cylinder is comprised of the piston, piston rings, and cylinder. It accounts for a significant amount of total engine friction within reciprocating, internal combustion engines. Reducing power cylinder friction is key to the development of efficient internal combustion engines. However, isolating individual power cylinder tribocouples for detailed analysis can be challenging. In this work, a new reciprocating liner test rig is developed and introduced. The rig design is novel, using a stationary piston and a reciprocating cylinder liner. Friction is calculated from the force measured in the connecting rod which supports the piston. The rig allows for independent control of peak cylinder pressure, speed, and lubricant temperature. Using the newly developed test rig, several technologies for friction reduction are evaluated and compared.

This paper describes a new method for measuring oil consumption using laser induced breakdown spectroscopy (LIBS). LIBS focuses a high energy laser pulse on a sample to form a transient plasma. As the plasma cools, each element produces atomic emission lines which can be used to identify and quantify the elements present in the original sample. In this work, a LIBS system was used on simulated engine exhaust with a focus on quantifying the inorganic components (termed ash) of the particulate emissions. Because some of the metallic elements in the ash almost exclusively result from lube oil consumption, their concentrations can also be correlated to an oil consumption rate. Initial testing was performed using SwRI’s Exhaust Composition Transient Operation Laboratory®(ECTO-Lab®) burner system so that oil consumption and ash mass could be precisely controlled.

Gasoline direction injection (GDI) engines have been widely used by light-duty vehicle manufacturers in recent years to meet stringent fuel economy and emissions standards. Particulate Matter (PM) mass emissions from current GDI engines are primarily composed of soot particles or black carbon with a small fraction (15% to 20%) of semi-volatile hydrocarbons generated from unburned/partially burned fuel and lubricating oil. Between 2017 and 2025, PM mass emissions regulations in the USA are expected to become progressively more stringent going down from current level of 6 mg/mile to 1 mg/mile in 2025. As PM emissions are reduced through soot reduction, lubricating oil derived semi-volatile PM is expected to become a bigger fraction of total PM mass emissions.

Semi-volatile organic compounds (SVOC) are a group of compounds in engine exhaust that either form during combustion or are part of the fuel and lubricating oil. Since these compounds occur at very low concentrations in diesel engine exhaust, the methods for sampling, handling, and analyzing these compounds are critical to obtaining good results. An improved dilute exhaust sampling method was used for sampling and analyzing SVOC in engine exhaust, and this method was performed during transient engine operation. A total of 22 different SVOC were measured using a 2012 medium-duty diesel engine. This engine was equipped with a stock diesel oxidation catalyst (DOC), a diesel particulate filter (DPF), and a selective catalytic reduction (SCR) catalyst in series. Exhaust concentrations for SVOC were compared both with and without exhaust aftertreatment. Concentrations for the engine-out SVOC were significantly higher than with the aftertreatment present.

Fuel economy is not an absolute attribute, but is highly dependent on the method used to evaluate it. In this work, two test methods are used to evaluate the differences in fuel economy brought about by changes in engine oil viscosity grade and additive chemistry. The two test methods include a chassis dynamometer vehicle test and an engine dynamometer test. The vehicle testing was conducted using the Federal Test Procedure (FTP) testing protocol while the engine dynamometer test uses the proposed American Society for Testing and Materials (ASTM) Sequence VIE fuel economy improvement 1 (FEI1) testing methodology. In an effort to improve agreement between the two testing methods, the same model engine was used in both test methods, the General Motors (GM) 3.6 L V6 (used in the 2012 model year Chevrolet™ Malibu™ engine). Within the lubricant industry, this choice of engine is reinforced because it has been selected for use in the proposed Sequence VIE fuel economy test.

With the impending development of GF-6, the newest generation of engine oil, a new standardized oil oxidation and piston deposit test was developed using Chrysler 3.6 L Pentastar engine. The performance requirements and approval for passenger car light duty gasoline engine oil categories are set by the International Lubricants Standardization and Approval committee (ILSAC) and the American Petroleum Institute (API) using standardized testing protocols developed under the guidance of ASTM, the American Society for Testing and Materials. This paper describes the development of a new ASTM Chrysler oxidation and deposit test that will be used to evaluate lubricants performance for oil thickening and viscosity increase, and piston deposits.

Semi-volatile organic compounds (SVOC) are a group of compounds that may form during combustion and/or are present in the unburned portion of the fuel and lubricating oil which ultimately become part of the exhaust. Many of these compounds are considered toxic or carcinogenic. Since these compounds are present in very low concentrations in diesel engine exhaust, the methods for sampling, handling, and analyzing these compounds are critical to obtaining representative and repeatable results. Engine testing is typically performed using a dilution tunnel. With a dilution tunnel, the collection of a representative sample is important. Experiments were performed with a modified EPA Method TO-9A to determine the equilibration time and other sampling parameters required for the measurement of SVOC in dilute exhaust. The results show that representative results can be obtained with this method.

Dual fuel engines have shown significant potential as high efficiency powerplants. In one example, SwRI® has run a high EGR, dual-fuel engine using gasoline as the main fuel and diesel as the ignition source, achieving high thermal efficiencies with near zero NOx and smoke emissions. However, assuming a tank size that could be reasonably packaged, the diesel fuel tank would need to be refilled often due to the relatively high fraction of diesel required. To reduce the refill interval, SwRI investigated various alternative fluids as potential ignition sources. The fluids included: Ultra Low Sulfur Diesel (ULSD), Biodiesel, NORPAR (a commercially available mixture of normal paraffins: n-pentadecane (normal C15H32), and n-hexadecane (normal C16H34)) and ashless lubrication oil. Lubrication oil was considered due to its high cetane number (CN) and high viscosity, hence high ignitability.

A solid particle sampling system (SPSS) that is equipped with a heated oxidation catalyst, micro-dilution tunnels, filter holders and sampling probes, was designed and developed to collect filter-based solid and total (solid plus volatile) particles from the exhaust of internal combustion engines, and to facilitate the measurement of solid and total particles when equipped with particle measuring instruments for size, number, mass, and other particle characteristics. The SPSS was characterized with laboratory aerosol and showed a very low solid particle loss of less than 5 percent using sodium chloride particles, very high volatile particle removal of better than 98 percent using oil droplets, and no formation of sulfuric acid particles when using ammonium sulfate particles. The SPSS is a useful tool for researchers interested in characterizing the solid and volatile fraction of particles emitted from combustion sources.

The Oil Certification Committee of the National Marine Manufacturers Association has developed FC-W®, a new standard for crankcase lube oil used in four-stroke cycle inboard, outboard, and sterndrive marine engines. A sub-committee representing the marine engine industry, the oil industry, oil testing laboratories, and the NMMA engineering standards group was formed to study the lubrication and corrosion prevention needs of four-stroke cycle engines. The sub-committee developed a rust test and an engine test as well as adopting 3 industry standard bench tests. These tests, together with formulation restrictions are used to identify oils that meet the requirements for use in four-stroke cycle marine engines. This paper gives an overview of the development of the new tests, formulation restrictions, and product approval system.

Cabin air quality is of continuing importance [1]. Contamination of air with particulates or vapors has the potential of affecting the health of passengers and flight crew. Therefore, measures are required to maintain acceptable levels of cabin air quality. One potential source of cabin air contamination is lubricating oils used in the engines. Type II oils are required for the main engines, but Type I or Type II oils can be used for the APU, with Type I recommended by some engine manufacturers for its cold-start properties. Southwest Research Institutes (SwRI®) Department of Emissions Research used an internally developed analytical method called Direct Filter Injection/Gas Chromatograph (DFI/GC™) to analyze for volatile fractions of lubricating oil contaminants on Environmental Control System (ECS) components. Samples of two standard Type II aviation turbine lubricating oils were analyzed with the DFI/GC™ method and their spectra examined.

Engine tests are widely used to measure the ability of lubricating oils to reduce fuel consumption through improved mechanical efficiency. Previous publications have correlated laboratory-scale tests with the well-established Sequence VI and VIA engine methods. The present paper uses a matrix of 66 oils to produce an empirical model for the recently developed Sequence VIB engine test. A smaller matrix of oils was available for correlation with Sequence VI and VIA results. The models combine a purposely-designed friction test with conventional measures of kinematic and high-temperature high-shear viscosity. Good correlation was obtained with the Sequence VI, VIA and VIB results, as well as each of the five stages in the Sequence VIB test. The effects of lubricant oxidation in the 96-hour FEI-2 portion of the Sequence VIB test were similar for each of the oils. As a result, good correlation was observed between FEI-1 and FEI-2 results from the VIB test.

The Partnership for a New Generation Vehicle (PNGV) has identified the compression-ignition, direct-injection (CIDI) engine as a promising technology in meeting the PNGV goal of 80 miles per gallon for a prototype mid-size sedan by 2004. Challenges remain in reducing the emission levels of the CIDI-engine to meet future emission standards. The objective of this project was to perform an initial screening of crank case lubricant contribution to regulated engine-out emissions, particularly when low particulate forming diesel fuel formulations are used. The test engine was the Mercedes-Benz OM611, the test oils were a mineral SAE 5W30, a synthetic (PAO based) SAE 5W30, and a synthetic (PAO based) SAE 15W50, and the test fuels were a California-like certification fuel and an alternative oxygenated diesel fuel.

The specific goal of this project was to determine if there is a difference in the lube oil degradation rates in a heavy-duty diesel engine equipped with an EGR system, as compared to the same configuration of the engine, but minus the EGR system. A secondary goal was to develop FTIR analysis of used lube oil as a sensitive technique for rapid evaluation of the degradation properties of lubricants. The test engine selected for this work was a Caterpillar 3176 engine. Two engine configurations were used, a standard 1994 design and a 1994 configuration with EGR designed to meet the 2004 emissions standards. The most significant changes in the lubricant occurred during the first 50-100 hours of operation. The results clearly demonstrated that the use of EGR has a significant impact on the degradation of the engine lubricant.

This paper presents a discussion on manual transmission torque losses and focuses specifically on the relationship between torque loss, input speed and torque. It also includes a discussion on other factors affecting torque loss, such as inclination angle and lube oil temperature. Manual transmissions used in compact light truck applications have torque losses that are a function of input speed and torque. Efficiency studies done on manual transmissions in the engine-driving mode indicate that torque losses, in other than direct-drive gears, are considerably more dependent on input torque than input speed. It was also observed that efficiency was significantly affected by the inclination angle and lube oil temperature.

The contribution of lubricating oil to diesel engine particulate emissions is of concern not only because of stringent particulate emissions standards but also because of engine-to-engine variability. Unburned oil contributes directly to the particulate soluble organic fraction. A real-time oil consumption measurement technique previously developed was further refined to also measure real-time unburned oil consumption. The technique uses high sulfur oil, low sulfur fuel, and fast response, sensitive SO2 detection instrumentation. Total and unburned oil consumption maps over the engine operating range are presented. Results show that both total and unburned oil consumption generally increase as speed and load are increased. Unburned oil consumption shows some peaks at intermediate speed, high-load conditions. Oil consumption from individual cylinders was measured and shown to be approximately equal.

A Single Cylinder Medium Speed diesel engine research facility has been developed for investigating areas of current technical concern to the rail, marine and stationary power industries. The design and operation of this Single Cylinder Research Engine (SCRE) is described. The facility is centered around a Bombardier model 251-plus 11.0 L engine which is representative of four stroke multi-cylinder railroad, marine and small stationary powerplant engines. All engine support systems (air, cooling water, fuel oil and lubricating oil pumps) operate independent of the engine enabling a wide range of adjustments in flow, pressure and temperature. Current program areas for which this system is used include alternative fuels evaluation, combustion analyses, fuel injection system development, component wear and durability studies, engine friction analyses, lubricant testing and emissions evaluations.