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Due to its potential for simultaneous improvement in fuel consumption and exhaust emissions, controlled autoignition (CAI) combustion has been subject to continuous research in the last several years. At the same time, there has been a lot of interest in the use of alternative fuels in order to reduce reliance on conventional fossil fuels. Therefore, this experimental study has been carried out to investigate the effect of alcohol fuels on the CAI combustion process and on the resulting engine performance. The experimental work was conducted on an optical single cylinder engine with an air-assisted injector. To achieve controlled autoignition, residual gas was trapped in the cylinder by using negative valve overlap and an intake air heater was used to ensure stable CAI combustion in the optical engine. Methanol, ethanol and blended fuels were tested and compared with the results of gasoline.