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As a new method to examine the extremely unsteady and spatially varying wall heat transfer phenomena on diesel engine combustion chamber wall, high-speed imaging of infrared thermal radiation from the chromium coated window surface impinged by a diesel spray flame has been conducted in a constant volume combustion chamber. The infrared radiation from a back surface of the chromium layer was successfully visualized at 10kHz frame rate and 128 × 128 pixel resolution through the window. The distributions of infrared radiation, temperature and heat flux exhibited coherent and streaky structure with radial stripes extending and waving from a stagnation point likely reflecting the near-wall turbulent structure in a wall impinging diesel flame. The experiments were conducted with various parameters such as fuel injection pressure, ambient gas oxygen concentration, wall impinging distance, wall surface roughness and wall materials.

The enhancement of vortex development, fuel-air mixing and heat release in diesel spray flame by inversed-delta injection rate shaping, having been predicted via LES simulation with detailed chemical kinetics, is experimentally confirmed for the first time. Newly developed 3-injector TAIZAC (TAndem Injector Zapping ACtivation) injector realizing aggressive inversed-delta injection rate shaping was used for single-shot combustion experiments in a constant volume combustion vessel. Simultaneous high-speed (120,000fps) and high-resolution (1,280 x 704 pixels) laser schlieren and UV OH* chemiluminescence imaging combined with subsequent Flame Imaging Velocimetry (FIV) analysis was employed to elucidate the correlation between vortex development and enhanced heat release.

In order to explore the potential of thermal efficiency improvement of diesel engines with injection rate shaping, TAIZAC (TAndem Injectors Zapping ACtivation) injector consisting of commercially available two common-rail injectors was developed in-house. A simple architecture adopted for TAIZAC injector consists of an upper injector connected to a high pressure source, a lower injector injecting into the cylinder and sealing parts between the two injectors. A fast response piezo-actuated injector (G3P) was employed as the upper one with an additionally drilled large axial orifice for faster fuel supply. A solenoid-actuated injector (G4S) was employed as the lower one for its applicability to inner volume reduction by body cut.

For better understanding, model development and its validation of in-cylinder soot formation processes of Gasoline Direct Injection (GDI) engines, crank-angle-resolved mass and size distribution of in-cylinder soot during a GDI combustion cycle were investigated via optical measurements and total cylinder sampling technique in an optically accessible Rapid Compression and Expansion Machine (RCEM). A direct-injection, spark-ignited and single-shot combustion event was achieved in the RCEM operated with engine speed 600 rpm, compression ratio 9.0, equivalence ratio 0.9 and natural aspiration. A three-component (iso-octane 65%, n-heptane 10%, toluene 25%) gasoline surrogate fuel and a multi-hole injector shared within the Japanese SIP Innovative Combustion Technology research program were used.

A mixed timescale subgrid model of a large eddy simulation was used to simulate the turbulence regime in diesel engine combustion. The combustion model used the direct integration approach with a diesel oil surrogate mechanism (developed at Chalmers University of Technology and consisting of 70 species and 309 reactions). Additional reactions for the generation and consumption of OH*, CO2*, and CH* species were added from recent kinetic studies. Collisional quenching and spontaneous emission resulted in de-excitation of the excited state radical. A phenomenological soot formation model (developed at Waseda University) was combined with the LES code. The following important steps were considered in the soot model: particle inception where naphthalene grows irreversibly to form soot, surface growth with the addition of C2H2, surface oxidation (induced by OH radicals and O2 attack), and particle coagulation.

In our previous work, diesel late combustion heat release is suspected to originate from rich fuel mixture cloud stagnating at the spray tip. Injection rate shaping is gaining attention as an attractive strategy to control diesel spray combustion characteristics where it could be an effective approach in reducing the late combustion. Progressive ramp-down injection rate as in “inversed-delta” shape is achieved by using a novel rate shaping injector called TAIZAC (TAndem Injectors Zapping Activation); rate shaping can be realized by controlling the actuation timing of two directly-connected commercially available injectors. To investigate the potential of inversed-delta rate shaping for reduction of diesel late combustion, simultaneous high-speed UV laser diffuse back illumination (DBI), UV emissions and soot luminosity imaging of inversed-delta and conventional rectangle-injected spray flames conducted in a constant volume combustion chamber are compared.

In order to better understand in-flame diesel soot oxidation processes, soot particles at the oxidation-dominant periphery of diesel spray flame were sampled by a newly developed “suck” type soot sampler employing a high-speed solenoid valve and their morphology and nanostructure were observed via high-resolution transmission electron microscopy (HR-TEM). A single-shot diesel spray flame for the soot sampling experiment was achieved in a constant-volume vessel under a diesel-like condition. The sampler instantaneously sucks out a small portion of soot laden gases from the flame. A TEM grid holds inside the flow passage close to its entrance is immediately exposed to the gas flow induced by the suction at the upstream of the solenoid valve, so that the quick thermophoretic soot deposition onto the grid surface can effectively freeze morphology variation of soot particles during the sampling processes.

In order to examine the effect of fuel aromatics on soot processes in diesel flame, nanostructure and morphology of soot particles directly sampled in a diesel flame were investigated via High-Resolution Transmission Electron Microscopy (HRTEM). Three test fuels with different aromatic contents, aromatic-free Fischer-Tropsch Diesel (FTD), naphthalene-added (65,000ppm) FTD and conventional JIS#2 diesel fuels were used. TEM grids were directly exposed to single-shot diesel flames in a constant volume combustion chamber under a diesel-like condition with EGR (1000K, 2.7MPa, 15%O2) to thermophoretically sample soot particles at different axial locations from 40 to 120mm from nozzle. The soot nanostructure such as length, tortuosity and separation of lattice fringes in primary particles and morphology such as primary particle diameter and aggregate gyration radius were analyzed and compared among different fuels and in-flame locations.

For better understanding of soot formation and oxidation processes in a diesel spray flame, two kinds of planar soot imaging techniques, Laser-Induced Incandescence (LII) and Laser Scattering (LS) techniques, were applied simultaneously to a diesel spray flame in a constant-volume combustion vessel under a diesel-like condition (2.5MPa, 940K). An analysis of LII and LS images yielded 2-dimensional distribution images of concentration, size and number density of soot particles in the spray flame, based on an assumption that LII and LS signals are proportional to the soot particle size to the power of 3 and 6, respectively. In order to obtain clearer variation trend in the soot concentration, size and number density distribution in significantly fluctuating single-shot diesel spray flames, spontaneous and time-integrated ensemble averaging of the laser-measured images were employed.

In order to examine the effect of aromatic addition to Fischer-Tropsch Diesel (FTD) fuel on formation and oxidation processes of soot particles in diesel spray flame, small amount of naphthalene (0 to 65,000 ppm) was added to the FTD fuel and variation of soot morphology and nanostructure of primary soot particles directly sampled in a diesel spray flame were investigated via High-Resolution Transmission Electron Microscopy (HRTEM). A single-shot diesel spray flame was achieved in a constant volume combustion chamber under a diesel-like condition (Ta=1000K, Pa=2.7MPa) and a grid for HRTEM observation was directly exposed to the spray flame to thermophoretically sample soot particles onto the grid surface. The primary particle diameter, aggregate gyration radius, lattice fringe length, lattice fringe tortuosity and lattice fringe separation of soot particles sampled at different locations (from 60 to 90mm from nozzle tip) in the spray flame were analyzed.

In-flame soot sampling based on the thermophoresis of particles and subsequent transmission electron microscope (TEM) imaging has been conducted in a diesel engine to study size, shape and structure of soot particles within the reacting diesel jet. A direct TEM sampling is pursued, as opposed to exhaust sampling, to gain fundamental insight about the structure of soot during key formation and oxidation stages. The size and shape of soot particles aggregate structure with stretched chains of spherical-like primary particles is currently an unknown for engine soot modelling approaches. However, the in-flame sampling of soot particles in the engine poses significant challenges in order to extract meaningful data. In this paper, the engine modification to address the challenges of high-pressure sealing and avoiding interference with moving valves and piston are discussed in detail.

For better understanding of soot formation and oxidation processes in diesel spray flame, the nanostructure of primary soot particles directly sampled in a diesel spray flame was investigated via High-Resolution Transmission Electron Microscopy (HRTEM). A single-shot diesel spray flame was achieved in a constant volume combustion vessel under diesel-like conditions (Ta=1000K, Pa=2.7 MPa) and a micro-grid for HRTEM observation was directly exposed to the spray flame to thermophoretically sample soot particles onto the grid surface. A preliminary nanostructure investigation was conducted for x500k magnification HRTEM images of soot particles directly sampled in diesel spray flames of Fischer-Tropsch Diesel (FTD) fuel seeded with naphthalene as a representative aromatic substance. A MATLAB code for HRTEM image processing and analysis of lattice fringes within primary soot particles was developed and used to characterize the length, tortuosity and separation of lattice fringes.

For a better understanding of soot formation and oxidation processes in conventional diesel and biodiesel spray flames, the morphology, microstructure and sizes of soot particles directly sampled in spray flames fuelled with US#2 diesel and soy-methyl ester were investigated using transmission electron microscopy (TEM). The soot samples were taken at 50mm from the injector nozzle, which corresponds to the peak soot location in the spray flames. The spray flames were generated in a constant-volume combustion chamber under a diesel-like high pressure and high temperature condition (6.7MPa, 1000K). Direct sampling permits a more direct assessment of soot as it is formed and oxidized in the flame, as opposed to exhaust PM measurements. Density of sampled soot particles, diameter of primary particles, size (gyration radius) and compactness (fractal dimension) of soot aggregates were analyzed and compared. No analysis of the soot micro-structure was made.