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Low temperature combustion is a promising way to reach low NOx emissions in Diesel engines but one of its drawbacks, in comparison to conventional Diesel combustion is the drastic increase of Unburned Hydrocarbons (UHC). In this study, the sources of UHC of a low temperature combustion system were investigated in both a standard, all-metal single-cylinder Diesel engine and an equivalent optically-accessible engine. The investigations were conducted under low load operating conditions (2 and 4 bar IMEP). Two piston bowl geometries were tested: a wall-guided and a more conventional Diesel chamber geometry. Engine parameters such as the start of injection (SOI) timing, the level of charge dilution via exhaust gas re-circulation (EGR), intake temperature, injection pressure and engine coolant temperature were varied. Furthermore, the level of swirl and the diameter of the injector nozzle holes were also varied in order to determine and quantify the sources of UHC.