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Inside an automobile, hundreds of connectors and electrical terminals in various locations experience different corrosive environments. These connectors and electrical terminals need to be corrosion-proof and provide a good electrical contact for a vehicle’s lifetime. Saltwater and sulfuric acid are some of the main corrosion concerns for these electrical terminals. Currently, various thin metallic layers such as gold (Au), silver (Ag), or tin (Sn) are plated with a nickel (Ni) layer on copper alloy (Cu) terminals to ensure reliable electrical conduction during service. Graphene due to its excellent chemical stability can serve as a corrosion protective layer and prevent electrochemical oxidation of metallic terminals. In this work, effects of thin graphene layers grown by plasma-enhanced chemical vapor deposition (PECVD) on Au and Ag terminals and thin-film devices were investigated. Various mechanical, thermal/humidity, and electrical tests were performed.

Nowadays, the increasing number of structural high pressure die casting (HPDC) aluminum parts need to be joined with high strength steel (HSS) parts in order to reduce the weight of vehicle for fuel-economy considerations. Self-Pierce Riveting (SPR) has become one of the strongest mechanical joining solutions used in automotive industry in the past several decades. Joining HPDC parts with HSS parts can potentially cause joint quality issues, such as joint button cracks, low corrosion resistance and low joint strength. The appropriate heat treatment will be suggested to improve SPR joint quality in terms of cracks reduction. But the heat treatment can also result in the blister issue and extra time and cost consumption for HPDC parts. The relationship between the microstructure of HPDC material before and after heat treatment with the joint quality is going to be investigated and discussed for interpretation of cracks initiation and propagation during riveting.

Fatigue damage prediction approaches in both time and frequency domains have been developed to simulate the operational life of mechanical structures under random loads. Fatigue assessment of mechanical structures and components subjected to those random loads is increasingly being addressed by frequency domain approaches because of time and cost savings. Current frequency-based fatigue prediction methods focus on stationary random loadings (stationary Power Spectral Density), but many machine components, such as jet engines, rotating machines, and tracked vehicles are subjected to non-stationary PSD conditions under real service loadings. This paper describes a new fatigue damage modeling approach capable of predicting fatigue damage for structures exposed to non-stationary (evolutionary) PSD loading conditions where the PSD frequency content is time-varying.

Driveline and suspension notched components of off-road ground vehicles often experience multiaxial fatigue failures along notch locations. Large nominal load histories may induce local elasto-plastic stress and strain responses at the critical notch locations. Fatigue life prediction of such notched components requires detailed knowledge of local stresses and strains at notch regions. The notched components that are often subject to multiaxial loadings in services, experience complex stress and strain responses. Fatigue life assessment of the components utilizing non-linear Finite Element Analysis (FEA) require unfeasibly inefficient computation times and large data. The lack of more efficient and effective methods of elasto-plastic stress-strain calculation may lead to the overdesign or earlier failures of the components or costly experiments and inefficient non-linear FEA.

Deep-hole drilling is among the most critical precision machining processes for production of high-performance discrete components. The effects of drilling with superimposed, controlled low-frequency modulation - Modulation-Assisted Machining (MAM) - on the surface textures created in deep-hole drilling (ie, gun-drilling) are discussed. In MAM, the oscillation of the drill tool creates unique surface textures by altering the burnishing action typical in conventional drilling. The effects of modulation frequency and amplitude are investigated using a modulation device for single-flute gun-drilling on a computer-controlled lathe. The experimental results for the gun-drilling of titanium alloy with modulation are compared and contrasted with conventional gun-drilling. The chip morphology and surface textures are characterized over a range of modulation conditions, and a model for predicting the surface texture is presented. Implications for production gun-drilling are discussed.

The new devices and missions to achieve the aims of NASA's Science Mission Directorate (SMD) are creating increasingly demanding thermal environments and applications. In particular, the low conductance of metal-to-metal interfaces used in the thermal switches lengthen the cool-down phase and resource usage for spacecraft instruments. During this work, we developed and tested a vacuum-compatible, durable, heat-conduction interface that employs carbon nanotube (CNT) arrays directly anchored on the mating metal surfaces via microwave plasma-enhanced, chemical vapor deposition (PECVD). We demonstrated that CNT-based thermal interface materials have the potential to exceed the performance of currently available options for thermal switches and other applications.

When high-intensity discharge (HID) electric lamps are used for plant growth, system inefficiencies occur due to an inability to effectively target light to all photosynthetic tissues of a growing crop stand, especially when it is closed with respect to light penetration. To maintain acceptable crop productivity, light levels typically are increased thus increasing heat loads on the plants. Evapotranspiration (ET) or transparent thermal barrier systems are subsequently required to maintain thermal balance, and power-intensive condensers are used to recover the evaporated water for reuse in closed systems. By accurately targeting light to plant tissues, electric lamps can be operated at lower power settings and produce less heat. With lower power and heat loads, less energy is used for plant growth, and possibly less water is evapotranspired. By combining these effects, a considerable energy savings is possible.

Three replicate aerobic-heterotrophic biotrickling filters were designed to promote the simultaneous biodegradation of graywater and a waste gas containing NH3, H2S and CO2. Upon visual observation of discolored solids, it was originally hypothesized that gas-phase CO2 concentrations were excessive, causing regions of anoxic zones to form within the biotrickling filters. Observed discolored (black) biofilm of this nature is typically assumed to be either lysed bacterial cells or anaerobic regions, implying alteration of operational conditions. Solid (biofilm) samples were collected in the presence and absence of gas-phase wastestream(s) to determine if the gas-phase contaminants were contributing to the solid-phase discoloration. Two sets of experiments (shaker flask and solids characterization) were conduced to determine the nature of the discolored solids. Results indicated that the discolored solids were neither anaerobic bacteria nor lysed cells.

Most of the gaseous contaminants generated inside ALS (Advanced Life Support) cabins can be degraded to some degree by microbial degradation in a biofilter. The entry of biofiltration techniques into ALS will most likely involve integration with existing physico-chemical methods. However, in this study, cabin air quality treated by only biofiltration was predicted using the one-box and biofiltration models. Based on BVAD (Baseline Values and Assumptions Document) and SMAC (Spacecraft Maximum Allowable Concentrations), ammonia and carbon monoxide will be the critical compounds for biofilter design and control. Experimentation is needed to identify the pertinent microbial parameters and removal efficiency of carbon monoxide and to validate the results of this preliminary investigation.

The Bioregenerative Air Treatment for Health system has been proposed for Advanced Life Support (ALS) planetary base applications. The system will be operated as a biotrickling filter to simultaneously treat graywater and waste gas. Preliminary experiments have focused on carbon removal from a graywater simulant. Six bench scale biotrickling filter reactors were constructed and monitored continuously. After a reactor startup phase of 40 days, the average total organic carbon (TOC) removal for reactors packed with Tri-packs® packing material was 62%. A second set of experiments was designed to evaluate TOC removal using different packing materials (Bee-cell and Biobale). It was hypothesized that the alternative packing materials would reduce the effects of channeling in the reactors, thus improving TOC removal. However, TOC removal did not significantly improve during the second set of experiments.

Resource recovery, including that of urine water extraction, is one of the most crucial aspects of long-term life support in interplanetary space travel. This paper will consequently examine an innovative approach to processing raw, undiluted urine based on low-temperature freezing. This strategy is uniquely different from NASA's current emphasis on either ‘integrated’ (co-treatment of mixed urine, grey, and condensate waters) or ‘high-temperature’ (i.e., VCD [vapor compression distillation] or VPCAR [vapor phase catalytic ammonia removal]) processing strategies, whereby this liquid freeze-thaw (LiFT) procedure would avoid both chemical and microbial cross-contamination concerns while at the same time securing highly desirable reductions in likely ESM levels.

The application of biological treatment to solid waste is very promising to facilitate recycling of water, carbon, and nutrients and to reduce the resupply needs of long-term crewed space missions. Degradation of biodegradable solid wastes generated during such a mission is under investigation as part of the NASA Center of Research and Training (NSCORT) at Purdue University. Processing in the solids thermophilic aerobic reactor (STAR) involves the use of high temperature micro-aerobic slurry conditions to degrade solid wastes, enabling the recycling of water, carbon, and nutrients for further downstream uses. Related research presently underway includes technical development and optimization of STAR operations as well as a complementary evaluation of post-STAR processing for gas-stream purification, water recovery by condensate purification, and residuals utilization for both mushroom growth media and nutritional support for fish growth.

Complete reuse of graywater will be essential during long duration human space missions. The highest loaded and most important component to remove from graywater is surfactant, the active ingredient in soaps and detergents. When considering a biological treatment system for processing of graywater, surfactant biodegradability becomes a very important consideration. Surfactants should be chosen that are degraded at a fast rate and yield inconsequential degradation byproducts. Experiments conducted for this research examined the biodegradation of the surfactants in Pert Plus for Kids, disodium cocoamphodiacetate (DSCADA) and sodium laureth-3 sulfate (SLES), using respirometry. Rates of CO2 production, or ultimate degradation, are reported. DSCADA was found to be toxic to bacteria when present at 270 ppm whereas no toxicity was observed during experiments with SLES.

The damping effect that is observed when a fibrous acoustical treatment is applied to a thin metal panel typical of automotive structures has been modeled by using three independent techniques. In the first two methods the fibrous treatment was modeled by using the limp frame formulation proposed by Bolton et al., while the third method makes use of a general poro-elastic model based on the Biot theory. All three methods have been found to provide consistent predictions that are in excellent agreement with one another. An examination of the numerical results shows that the structural damping effect results primarily from the suppression of the nearfield acoustical motion within the fibrous treatment, that motion being closely coupled with the vibration of the base panel. The observed damping effect is similar in magnitude to that provided by constrained layer dampers having the same mass per unit area as the fibrous layer.

The objective of this project is to quantify structural degradation due to corrosion through a fracture mechanics based approach. The metric parameters employed are Equivalent Initial Flaw Size and general material loss. Another objective is to correlate a measurable property to the amount of structural durability damage from corrosion, ideally through current NDE technology, with eddy-current as the primary choice. The approach is comprised by the following areas: corroding aluminum alloys, evaluation of the corrosion through techniques such as surface roughness and eddy current, cyclic testing, calculation of corrosion metric, and, correlation between corrosion metric and physically measurable properties.