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Technical Paper

Development of Titanium Nitride Coatings in Titanium Alloys by Electron Beam Physical Vapor Deposition

2008-10-07
2008-36-0016
It is observed an increasing interest in using titanium nitride (TiN) coatings to improve the wear properties of Ti alloys. An important method is the Electron Beam Physical Vapor Deposition (EBPVD) that is a form of deposition in which a target anode is bombarded with an electron beam given off by a charged tungsten filament under high vacuum, producing a thin film in a substrate. In this work are presented results of the target and substrate production using Ti (C.P.), Ti-6Al-4V and Ti-13Nb-13Zr by powder metallurgy. Samples were produced by mixing of initial metallic powders followed by uniaxial and cold isostatic pressing with subsequent densification by sintering between 900 to 1500 °C, in vacuum. Sintered samples were characterized for phase composition, microstructure and microhardness by X-ray diffraction, scanning electron microscopy and Vickers indentation, respectively. It was shown that the samples were sintered to high densities and presented homogeneous microstructure.
Technical Paper

Development of titanium alloys production for high temperatures applications.

2010-10-06
2010-36-0170
Turbine blades for airplanes work in adverse conditions, under corrosive environment and high temperatures and pressure conditions. Ti-6Al-2Sn-4Zr-2Mo alloy was developed for high temperatures applications in aerospace area. In this work, Ti-6Al-2Sn-4Zr-2Mo alloy was obtained by powder metallurgy using titanium hydride powders. Samples were manufactured by blended elemental method from a sequence of uniaxial and cold isostatic pressing with subsequent densification by sintering among 800 up to 1400°C, in vacuum. The objective of this work is the analysis of microstructural evolution from the powders dissolution with the increase of the sintering temperature. The alloy was characterized by scanning electron microscopy, X-ray diffraction and Vickers microhardness measurement. Density was measured by Archimedes method.
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