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Among the alternative fuels, dimethyl ether (DME), one of the oxygenated fuels, attracts attention as an alternative fuel for the Diesel engine since the properties of the DME are fitted to the Diesel engine combustion and the know-how development has been made of the mass production of the DME from a natural gas. In this study, experiments were performed of ignition characteristics of the DME and Diesel fuel sprays injected by a D.I. Diesel injector into a high-pressure, high-temperature vessel. The fuel injection was made by a Bosch type injection system. A schlieren optical system was adopted for visualizing the ignition process as well as the vaporization process of the DME and Diesel fuel sprays. The ignition delay was measured by using a photo-sensor which had a sensitivity in the wavelength range from visible to ultraviolet. Pressure and temperature of the ambient air and the oxygen concentration of the ambient air were changed as experimental parameters.