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Increasing concern for air pollution together with the introduction of new types of fuels pose new challenges to the exhaust aftertreatment system for heavy-duty (HD) vehicles. For diesel-powered engines, emissions of particulate matter (PM) is one of the main drawbacks due to its effect on health. To mitigate the tailpipe emissions of PM, heavy-duty vehicles are since Euro V equipped with a diesel particulate filter (DPF). The accumulation of particles causes flow restriction resulting in fuel penalties and decreased vehicle performance. Understanding the properties of PM produced during engine operation is important for the development and optimized control of the DPF. This study has focused on assessing the reactivity of the PM by measuring the oxidation kinetics of the carbonaceous fraction. PM was sampled from two different heavy-duty engines during various test cycles.