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The objective of the study is to investigate the effect of current pulsation frequency on the weld bead microstructure, segregation and hardness of Hastelloy C-2000 weldments. Bead on Plate (BoP) welds were made by using Pulsed Current Gas Tungsten Arc Welding method (PCGTAW) at eleven different frequencies. The weld bead width and depth of penetration was measured with the help of Dinolite macro analyzer. The microstructure of weldments are further examined through optical microscope and Scanning Electron Microscopy (SEM) to identify the type of grain, grain coarsening and extent of the Heat Affected Zone (HAZ). The grain structure turn into finer and equiaxed in all cases and there was an optimum frequency range over which the significant grain refinement was observed. Microsegregation of alloying elements were computed with the aid of Energy Dispersive X-ray Spectroscopy (EDS). Vickers Hardness Tester was used to measure the hardness of the weld samples at ambient conditions.

The current work investigates the hot corrosion demeanour of Hastelloy X weldment produced with autogenous mode through key-hole plasma arc welding (K-PAW). The hot corrosion test has been performed for weldment in molten salt-1 (MS-1) (75 % Na2SO4 + 25 % V2O5) and molten salt-2 (MS-2) (75 % Na2SO4 + 20 % V2O5 + 5 % NaCl) circumstance for 25 hrs (25 cycles) at 900 °C. The MS-1 substrate of both base metal and weldment provided the lowest weight gain than the MS-2 substrate. The NaCl in the MS-2 causes severe hot corrosion on the substrate, whereas the absence of NaCl in MS-1 reduces the hot corrosion effects. The highest parabolic constant is observed for K-PAW weldment in MS-2 condition. The tendency of hot corrosion rate follows the order of, Base Metal MS-1 < K-PAW MS-1 < Base Metal MS-2 < K-PAW MS-2. The occurrence of protective phases like chromium oxides (Cr2O3), spinel oxides (NiCr2O4 and NiFe2O4) Nickel oxide (NiO) on the substrate resist the further oxidation.

Duplex stainless steel (DSS) 2205 grade is welded with austenitic filler wires (ERNiCrMo-3 and ERNiCrMo-4) using gas tungsten arc welding (GTAW) process to operate at marine environments. Microstructure using optical (OM) and scanning electron microscopes (SEM) with energy dispersive spectroscope (EDS) are utilized to examine the metallurgical characterization of DSS 2205 weldments. Microhardness, impact, and tensile tests are employed to obtain the mechanical properties of weldments. Secondary precipitates such as Mo23C6 and Cr23C6 are formed in the ERNiCrMo-3 weldment which reduced the mechanical properties. In this study, ERNiCrMo-4 filler wire is provided enhanced mechanical properties for welding DSS 2205.