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Current demands for high fuel efficiency and low emissions in automotive powerplants have drawn attention to the two-stroke engine configuration. The present study measured trapping and scavenging efficiencies of a firing two-stroke spark-ignition engine by in-cylinder gas composition analysis. Intermediate results of the procedure included the trapped air-fuel ratio and residual exhaust gas fraction. Samples, acquired with a fast-acting electromagnetic valve installed in the cylinder head, were taken of the unburned mixture without fuel injection and of the burned gases prior to exhaust port opening, at engine speeds of 1000 to 3000 rpm and at 10 to 100% of full load. A semi-empirical, zero-dimensional scavenging model was developed based on modification of the non-isothermal, perfect-mixing model. Comparison to the experimental data shows good agreement.