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A new experimental methodology has been developed to quantify spindle loads of a vehicle under actual operational conditions. The methodology applies an indirect six degree-of-freedom (6 DOF) frequency response function (FRF) measurement technique to obtain three translation/force and three rotation/moment FRFs of the suspension system of the vehicle. The Inverse Frequency Response Function (IFRF) method estimates the spindle loads under operational conditions. The feasibility and applicability of the developed methodology for vehicle road NVH applications was experimentally demonstrated. The results show that the methodology provides accurate spindle load estimation over a broad frequency range. This methodology can be used for benchmarking and target setting of spindle loads to achieve desired road NVH performance as well as for diagnosing root causes in problem solving applications.