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To meet the future stringent emission standards, innovative diesel engine technology, exhaust gas after-treatment, and clean alternative fuels are required. Oxygenated fuels have showed a tendency to decrease internal combustion engine emissions. In the same time, advanced fuel injection modes can promote a further reduction of the pollutants at the exhaust without penalty for the combustion efficiency. One of the more interesting solutions is provided by the premixed low temperature combustion (LTC) mechanism jointly to lower-cetane, higher-volatility fuels. In this paper, to understand the role played by these factors on soot formation, cycle resolved visualization, UV-visible optical imaging and visible chemiluminescence were applied in an optically accessed high swirl multi-jets compression ignition engine. Combustion tests were carried out using three fuels: commercial diesel, a blend of 80% diesel with 20% gasoline (G20) and a blend of 80% diesel with 20% n-butanol (BU20).