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Phase separation is one of the most significant obstacles encountered during the development of analytical methods for water quality monitoring in spacecraft environments. Removing air bubbles from water samples prior to analysis is a routine task on earth; however, in the absence of gravity, this routine task becomes extremely difficult. This paper details the development and initial ground testing of liquid metering centrifuge sticks (LMCS), devices designed to collect and meter a known volume of bubble-free water in microgravity. The LMCS uses centrifugal force to eliminate entrapped air and reproducibly meter liquid sample volumes for analysis with Colorimetric Solid Phase Extraction (C-SPE). Previous flight experiments conducted in microgravity conditions aboard the NASA KC-135 aircraft demonstrated that the inability to collect and meter a known volume of water using a syringe was a limiting factor in the accuracy of C-SPE measurements.

Colorimetric-solid phase extraction (C-SPE) is being developed as a method for in-flight monitoring of spacecraft water quality. C-SPE is based on measuring the change in the diffuse reflectance spectrum of indicator disks following exposure to a water sample. Previous microgravity testing has shown that air bubbles suspended in water samples can cause uncertainty in the volume of liquid passed through the disks, leading to errors in the determination of water quality parameter concentrations. We report here the results of a recent series of C-9 microgravity experiments designed to evaluate manual manipulation as a means to collect bubble-free water samples of specified volumes from water sample bags containing up to 47% air. The effectiveness of manual manipulation was verified by comparing the results from C-SPE analyses of silver(I) and iodine performed in-flight using samples collected and debubbled in microgravity to those performed on-ground using bubble-free samples.

Providing water necessary to maintain life support has been accomplished in spacecraft vehicles for over forty years. This paper will investigate how previous U.S. space vehicles provided potable water. The water source for the spacecraft, biocide used to preserve the water on-orbit, water stowage methodology, materials, pumping mechanisms, on-orbit water requirements, and water temperature requirements will be discussed. Where available, the hardware used to provide the water and the general function of that hardware will also be detailed. The Crew Exploration Vehicle (CEV or Orion) water systems will be generically discussed to provide a glimpse of how similar they are to water systems in previous vehicles. Conclusions, questions, and recommendations on strategies that could be applied to CEV based on previous spacecraft water system lessons learned will be made.

Similar to finding a home on Earth, location is important when selecting where to set up an exploration outpost. Essential considerations for comparing potential lunar outpost locations include: (1) areas nearby that would be useful for In-Situ Resource Utilization (ISRU) oxygen extraction from regolith for crew breathing oxygen as well as other potential uses; (2) proximity to a suitable landing site; (3) availability of sunlight; (4) capability for line-of-sight communications with Earth; (5) proximity to permanently-shadowed areas for potential in-situ water ice; and (6) scientific interest. The Mons Malapert1 (Malapert Mountain) area (85.5°S, 0°E) has been compared to these criteria, and appears to be a suitable location for a lunar outpost.

A procedure for calculating the engine inlet diffuser section liquid water content and mass fractions of liquid water content associated with the water droplet size distribution for wind milling engine ice accretion analysis is presented. Critical fuel reserve calculation for extended twin-engine operation requires the determination of drag increase due to ice accretion on inoperative wind milling engine fan blade and guide vane.

A reliable nutrient delivery system is essential for long-term cultivation of plants in space. At the Kennedy Space Center, a series of ground-based tests are being conducted to compare candidate plant nutrient delivery systems for space. To date, our major focus has concentrated on the Porous Tube Plant Nutrient Delivery System, the ASTROCULTURE™ System, and a zeoponic plant growth substrate. The merits of each system are based upon the performance of wheat supported over complete growth cycles. To varying degrees, each system supported wheat biomass production and showed distinct patterns for plant nutrient uptake and water use.

The recovery of potable water from waste water produced by humans in regenerative life support systems is essential for success of long-duration space missions. The Lunar-Mars Life Support Test Project (LMLSTP) Phase II test was performed to validate candidate technologies to support these missions. The test was conducted in the Crew and Thermal Systems Division (CTSD) Life Support Systems Integration Facility (LSSIF) at Johnson Space Center (JSC). Discussed in this paper are the water recovery system (WRS) results of this test. A crew of 4-persons participated in the test and lived in the LSSIF chamber for a duration of 30-days from June 12 to July 12, 1996. The crew had accommodations for personal hygiene, the air was regenerated for reuse, and the waste water was processed to potable and hygiene quality for reuse by the crew during this period. The waste water consisted of shower, laundry, handwash, urine and humidity condensate.

The removal of dissolved ions from waste water is essential for water repurification on long-term human space missions. Lynntech, Inc., has demonstrated a novel electrochemically driven purification method using tubulated bipolar ion exchange membranes for the separation of dissolved inorganic impurities as well as charged organic species from waste water. Generally, electrochemical separation methods have limited applications since they can only be applied to the purification of water that has a sufficiently high dissolved ion content to make the water conductive. The novel tubulated bipolar membranes composed of bilayers of oppositely charged ionically conducting polymers can be used to overcome this limitation. This paper deals with the scaling-up of such a device to increase the throughput to process about 100 liters of waste water per day. This is achieved by using stacks of tubulated bipolar membranes.

An integrated water recovery system was operated for 91 days in support of the Lunar Mars Life Support Test Project (LMLSTP) Phase III test. The system combined both biological and physical-chemical processes to treat a combined wastewater stream consisting of waste hygiene water, urine, and humidity condensate. Biological processes were used for primary degradation of organic material as well as for nitrification of ammonium in the wastewater. Physical-chemical systems removed inorganic salts from the water and provided post-treatment. The integrated system provided potable water to the crew throughout the test. This paper describes the water recovery system and reviews the performance of the system during the test.

An evaporative heat sink has been designed and built by AlliedSignal for NASA's Johnson Space Center. The unit is a demonstrator of a primary heat exchanger for NASA's prototype Crew Return Vehicle (CRV), designated the X-38. The primary heat exchanger is responsible for rejecting the heat produced by both the flight crew and the avionics. Spacecraft evaporative heat sinks utilize space vacuum as a resource to control the vapor pressure of a liquid. For the X-38, water has been chosen as the heat transport fluid. A portion of this coolant flow is bled off for use as the evaporant. At sufficiently low pressures, the water can be made to boil at temperatures approaching its freezing point. Heat transferred to liquid water in this state will cause the liquid to evaporate, thus creating a heat sink for the spacecraft's coolant loop. The CRV mission requires the heat exchanger to be compact and low in mass.

The International Space Station (ISS) recycles water to reduce the expense of launching water on resupply vehicles. However, since these recovery systems cannot recover 100% of all water used, some resupply is needed. Water consumption, as well as water recovery, varies from crew to crew making it difficult to judge how much water is needed and when. Therefore, the ground team tracks the water usage of the crew and determines a representative rate to predict each Expedition's water needs and identify trends in changing rates. This paper describes the analyses conducted to determine how much water each crew is using for drinking and hygiene purposes and how much is used for oxygen generation. It will also show how the water usage evolved over the last three Expeditions and compare these results to the published consumables tracking reports and the Russian water specialist reports.

Recovery of potable water from wastewater is essential for the success of long-term manned missions to the moon and Mars. Honeywell International and the team consisting of Thermodistillation Company (Kyiv, Ukraine) and NASA Johnson Space Center (JSC) Crew and Thermal Systems Division are developing a wastewater processing subsystem that is based on centrifugal vacuum distillation. The Wastewater Processing Cascade Distillation Subsystem (CDS) utilizes an innovative and efficient multi-stage thermodynamic process to produce purified water. The rotary centrifugal design of the system also provides gas/liquid phase separation and liquid transport under microgravity conditions. A five-stage prototype of the subsystem was built, delivered and integrated into the NASA JSC Advanced Water Recovery Systems Development Facility for development testing.

The Spacesuit Water Membrane Evaporator (SWME) is the baseline heat rejection technology selected for development for the Constellation lunar suit. The first SWME prototype, designed, built, and tested at Johnson Space Center in 1999 used a Teflon hydrophobic porous membrane sheet shaped into an annulus to provide cooling to the coolant loop through water evaporation to the vacuum of space. This present study describes the test methodology and planning to compare the test performance of three commercially available hollow fiber materials as alternatives to the sheet membrane prototype for SWME, in particular, a porous hydrophobic polypropylene, and two variants that employ ion exchange through non-porous hydrophilic modified Nafion. Contamination tests will be performed to probe for sensitivities of the candidate SWME elements to ordinary constituents that are expected to be found in the potable water provided by the vehicle, the target feedwater source.

In a crewed spacecraft environment, atmospheric carbon dioxide (CO2) and moisture control are crucial. Hamilton Sundstrand has developed a stable and efficient amine-based CO2 and water vapor sorbent, SA9T, that is well suited for use in a spacecraft environment. The sorbent is efficiently packaged in pressure-swing regenerable beds that are thermally linked to improve removal efficiency and minimize vehicle thermal loads. Flows are controlled with a single spool valve. This technology has been baselined for the new Orion spacecraft, but additional data was needed on the operational characteristics of the package in a simulated spacecraft environment. One unit was tested with simulated metabolic loads in a closed chamber at Johnson Space Center during the latter part of 2006. Those test results were reported in a 2007 ICES paper.

A system of amine-based carbon dioxide (CO2) and water vapor sorbent in pressure-swing regenerable beds has been developed by Hamilton Sundstrand and is baselined for the Orion Atmosphere Revitalization System (ARS). In two previous years at this conference, reports were presented on extensive Johnson Space Center (JSC) testing of the technology, which was performed in a representative environment with simulated human metabolic loads. The next step in developmental testing at JSC was to use real human loads in the spring of 2008.

One of the long-standing concerns in space exploration is the presence of trace organic contaminants in recycled spacecraft water supplies. At present, water samples on the International Space Station (ISS) are collected at regular intervals, stored in Teflon™-lined containers, and returned to Earth for characterization. This approach, while effective in defining water quality, has several notable problems. First, this method of archiving removes a significant volume of the ISS water supply. Second, the archived water consumes valuable cargo space in returning Shuttle and Soyuz vehicles. Third, the organic contaminants present in the collected samples may degrade upon extended storage. The latter problem clearly compromises sample integrity. Upon return to Earth, sample degradation is minimized by refrigeration. Due to present resource constraints, however, refrigeration is not a viable option in space.

A sorption-spectrophotometric platform for the concentration and subsequent quantification of biocides in spacecraft drinking water is described. This methodology, termed Colorimetric Solid Phase Extraction (C-SPE), is based on the extraction of analytes onto a membrane impregnated with a colorimetric reagent. Quantification of the extracted analytes is accomplished by interrogating the surface of the membrane with a commercially available diffuse reflectance spectrophotometer. Ground-based experiments have shown that C-SPE is a viable means to determine biocide concentrations in the range commonly found in water samples from the Space Shuttle and the International Space Station (ISS). This paper details efforts to advance C-SPE closer to space flight qualification and ISS implementation, starting with the modification of the ground based biocide detection platform to simplify operation in a microgravity environment.

The International Space Station (ISS) drinking water supply consists of water recovered from humidity condensate, water transferred from Shuttle, and groundwater supplied from Russia. The water is dispensed from both the stored water dispensing system (SVO-ZV) and the condensate recovery system (SRV-K) galley. Teflon bags are used periodically to collect potable water samples, which are then transferred to Shuttle for return to Earth. The results from analyses of these samples are used to monitor the potability of the drinking water on board and evaluate the efficiency of the water recovery system. This report provides results from detailed analyses of samples of ISS recovered potable water, Shuttle-supplied water, and ground-supplied water taken during ISS Expeditions 4 and 5. During Expedition 4, processing of U.S. Lab condensate through the Russian condensate recovery system was initiated. Results indicate water recovered from both Service Module and U.S.

The purification of waste water is a critical element of any long-duration space mission. The Vapor Phase Catalytic Ammonia Removal (VPCAR) system offers the promise of a technology requiring low quantities of expendable material that is suitable for exploration missions. NASA has funded an effort to produce an engineering development unit specifically targeted for integration into the NASA Johnson Space Center's Integrated Human Exploration Mission Simulation Facility (INTEGRITY) formally known in part as the Bioregenerative Planetary Life Support Test Complex (Bio-Plex) and the Advanced Water Recovery System Development Facility. The system includes a Wiped-Film Rotating-Disk (WFRD) evaporator redesigned with micro-gravity operation enhancements, which evaporates wastewater and produces water vapor with only volatile components as contaminants. Volatile contaminants, including organics and ammonia, are oxidized in a catalytic reactor while they are in the vapor phase.

The work presented in this paper summarizes the early results of an integrated advanced water recovery system test conducted by the Crew and Thermal Systems Division (CTSD) at NASA-Johnson Space Center (JSC). The system design and the results of the first two months of operation are presented. The overall objective of this test is to demonstrate the capability of an integrated advanced water recovery system to produce potable quality water for at least six months. Each subsystem is designed for operation in microgravity. The primary treatment system consists of a biological system for organic carbon and ammonia removal. Dissolved solids are removed by reverse osmosis and air evaporation systems. Finally, ion exchange technology in combination with photolysis or photocatalysis is used for polishing of the effluent water stream. The wastewater stream consists of urine and urine flush water, hygiene wastewater and a simulated humidity condensate.