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Technical Paper

Colorimetric-Solid Phase Extraction Technology for Water Quality Monitoring: Evaluation of C-SPE and Debubbling Methods in Microgravity

2007-07-09
2007-01-3217
Colorimetric-solid phase extraction (C-SPE) is being developed as a method for in-flight monitoring of spacecraft water quality. C-SPE is based on measuring the change in the diffuse reflectance spectrum of indicator disks following exposure to a water sample. Previous microgravity testing has shown that air bubbles suspended in water samples can cause uncertainty in the volume of liquid passed through the disks, leading to errors in the determination of water quality parameter concentrations. We report here the results of a recent series of C-9 microgravity experiments designed to evaluate manual manipulation as a means to collect bubble-free water samples of specified volumes from water sample bags containing up to 47% air. The effectiveness of manual manipulation was verified by comparing the results from C-SPE analyses of silver(I) and iodine performed in-flight using samples collected and debubbled in microgravity to those performed on-ground using bubble-free samples.
Technical Paper

Quantification of 3D Ice Structures Accreted on a Wind Turbine Airfoil Model

2019-06-10
2019-01-2030
Accurate quantification of 3D shapes of the complex ice structures accreted on wind turbine blades is highly desirable to develop ice prediction models for more accurate prediction of the aerodynamic performance degradation and power reduction due to the ice accretion on wind turbine blades. In the present study, an experimental investigation was conducted to quantitatively characterize the 3D shapes of the ice structures accreted over a DU91-W2-250 wind turbine airfoil model in the Icing Research Tunnel available at Iowa State University (ISU-IRT). A glaze icing condition and a rime icing condition that wind turbines usually experience in winter were duplicated by using ISU-IRT. A high-resolution non-intrusive 3D scanning system was used to make detailed 3D-shape measurements to quantify the complicated ice structures accreted on the wind turbine airfoil model as a function of the ice accretion time.
Technical Paper

An Experimental Study to Evaluate the Droplet Impinging Erosion Characteristics of an Icephobic, Elastic Soft Surface

2019-06-10
2019-01-1997
Elastic soft material/surface, such as Polydimethylsiloxane (PDMS), is a perspective, useful and low-cost hydrophobic and icephobic coating. While it has been reported to have good mechanical durability, its erosion durability under the high impacting of water droplets pertinent to aircraft inflight icing phenomena has not been explored. In this study, the droplet imping erosion characteristics of an icephobic PDMS surface/material is evaluated systematically upon the dynamic impinging of water droplets at different impact velocities (~ up to 75m/s), in comparison with other state-of-the-art icephobic materials/surfaces, such as superhydrophobic surface (SHS) and slippery liquid-infused porous surface (SLIPS). Surprisingly, the contact angle (CA) of the elastic PDMS is shown to have an over 20° increase (from 105° to 128°), which represents better hydrophobicity, after the erosion test which is mainly contributed to the higher roughness of the eroded PDMS surface.
Technical Paper

An Explorative Study to Use Super-Hydrophilic/Super-Hydrophobic Hybrid Surfaces for Aircraft Icing Mitigation

2019-06-10
2019-01-1995
An explorative study was performed to demonstrate the feasibility of using a novel hybrid anti-/de-icing strategy for aircraft icing mitigation. The hybrid method was developed by combining the electro-thermal heating mechanism and specialized surfaces/coatings with different wettabilities. While an electrical film heater was utilized to provide thermal energy around the leading edge of a NACA0012 airfoil model, two different coating strategies, (i.e., (a). Superhydrophobic coating covering the entire airfoil surface to increase droplets bounce-off and accelerate surface water runback vs. (b). super-hydrophilic coating at the leading edge to increase evaporation area + superhydrophobic coating in downstream to prevent runback refreezing) were proposed and evaluated aiming at maximizing the anti-/de-icing efficiency of the hybrid method.
Technical Paper

An Experimental Investigation of a Wind-Driven Water Droplet over the Slippery Liquid Infused Porous Surface

2019-06-10
2019-01-1951
The promising anti-icing performance of the slippery liquid infused porous surface (SLIPS) has been recently demonstrated for various engineering applications. The runback icing for aircraft and wind turbines could be effectively mitigated considering the timely removal of water droplet by the wind shearing force due to the low adhesion on the SLIPS. In this study, the flow field both inside and around the wind-driven droplet over the SLIPS was experimentally investigated by using Particle Image Velocimetry (PIV) technique. Previous studies majorly focus on the internal flow pattern before the droplet incipient motion. In this study, the flow field inside a moving droplet was firstly investigated. As a result of the low surface adhesion of the SLIPS, droplet oscillations were eliminated and the droplet internal flow field could be corrected from the optical distortion.
Technical Paper

Characterization of Mode-II Interfacial Fracture Toughness of Ice/Metal Interfaces

2019-06-10
2019-01-1947
Airborne, marine and ground structures are vulnerable to atmospheric icing in cold weather operation conditions. Most of the ice adhesion-related work have focused on the mechanical ice removal strategies because of practical considerations, while limited literature is available for fundamental understanding of the ice adhesion process. Here, we present a fracture mechanics-based approach to characterize interfacial fracture parameters for the shear behavior of a typical ice/aluminum interface. An experimental framework employing two complementary tests (1) lap shear and (2) shear push-out tests was introduced to assess the mode-II fracture parameters for the selected aluminum/ice interface. Both analytical (shear-lag analysis) and numerical (finite element analysis incorporating cohesive zone method) models were used to evaluate shear fracture parameters.
Technical Paper

A Parametric Study on the Thermodynamic Characteristics of DBD Plasma Actuation and Its Potential for Wind Turbine Icing Mitigation

2019-06-10
2019-01-2031
Wind turbine icing represents the most significant threat to the integrity of wind turbines in cold weather. Ice formation on wind turbine blades was found to cause significant aerodynamic performance degradation, resulting in a substantial drop in energy production. Recently developed Dielectric barrier discharge (DBD) plasma-based anti-/de-icing systems showed very promising effects for aircraft icing mitigation. In this present study, DBD plasma-based anti-/de-icing systems were employed for wind turbine icing mitigation. First, a comprehensive parametric study is conducted to investigate the effects of various DBD plasma actuation parameters on its thermodynamic characteristics. An infrared (IR) thermal imaging system is used to quantitatively measure the temperature distributions over the test plate under various test conditions.
Journal Article

Numerical and Experimental Investigation of Ice Adhesion Using the Blister Test

2019-06-10
2019-01-1948
Structures in cold weather environments are susceptible to atmospheric ice formation. A fracture mechanics based approach is proposed for in situ characterization of the interfacial fracture energy of ice on different substrates. This paper summarizes the development of the experimental and analytical framework to measure the ice adhesion energy, calibrated on static ice. The testing configuration utilizes a shaft-loaded blister test to produce stable crack propagation, from a well-defined pre-crack at the interface of the ice layer and the substrate. Measurements of the fracture energy are taken over a range of ice thicknesses and surface roughnesses. The developed analytical framework to estimate adhesion energy are verified and calibrated via finite element numerical simulation of the proposed geometric configuration and employing cohesive surfaces along the interface to simulate the crack nucleation and propagation process.
Journal Article

Modeling the Effects of Drop Impingement Frequency on Heated Walls at Engine Conditions

2022-03-29
2022-01-0508
Understanding the fundamental details of drop/wall interactions is important to improving engine performance. Most of the drop-wall interactions studies are based on the impact of a single drop on the wall. To accurately mimic and model the real engine conditions, it is necessary to characterize spray/wall interactions with different impingement frequencies at a wide range of wall temperatures. In this study, a numerical method, based on Smoothed Particle Hydrodynamics (SPH), is used to simulate consecutive droplet impacts on a heated wall both below and above the Leidenfrost temperature. Impact regimes are identified for various impact conditions by analyzing the time evolution of the post-impingement process of n-heptane drops at different impingement frequencies and wall surface temperatures. For wall temperature below the Leidenfrost temperature, the recoiled film does not leave the surface.
Journal Article

Microgravity Evaluation of Colorimetric-Solid Phase Extraction for the Measurement of Total I (Iodine, Iodide, and Triiodide) in Spacecraft Drinking Water

2008-06-29
2008-01-2199
We are developing a drinking water test kit based on colorimetric-solid phase extraction (C-SPE) for use onboard the International Space Station (ISS) and on future Lunar and/or Mars missions. C-SPE involves measuring the change in diffuse reflectance of indicator disks following their exposure to a water sample. We previously demonstrated the effectiveness of C-SPE in measuring iodine in microgravity. This analytical method has now been extended to encompass the measurement of total I (i.e., iodine, iodide, and triiodide). This objective was accomplished by introducing an oxidizing agent to convert iodide and triiodide to iodine, which is then measured using the indicator disks previously developed for iodine. We report here the results of a recent series of C-9 microgravity tests of this method. The results demonstrate that C-SPE technology is poised to meet the total I monitoring requirements of the international space program.
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