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Pure aluminium alloy (AA) components are not extending their cyclic life due to soft nature of the surfaces for most of the automotive structural parts, exposed to various loading and stress exposed areas through various surface property enhancement techniques. Among all the technique friction stir processing (FSP) followed by shot peening (SP) technique is the most viable and cost-effective process for enhancement of component performance and SP removing residual stresses on the samples thereby improving surface strength. The main objective of the proposed work was cast A356 alloy reinforced with nano form of 6wt% silicon carbide (SiC) harder particles and 3wt% self-lubricant graphene (Gr) was used to fabricated a surface nano hybrid composite through FSP technique. SP route was performed on the FSP-ed samples with optimal parametric conditions for obtaining improved mechanical performances.