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Due to the reduced or less-frequent usages of the friction brakes and the lower brake rotor temperature on electrical vehicles (EV), corrosion would much likely occur on brake rotors. Using hard braking to clean the corroded rotor surfaces often leads to extra rotor surface wear. Improvement in corrosion and wear resistance is an important technological topic to brake rotors for EVs. Many original equipment manufacturers (OEM) and their suppliers are exploring surface treatments including laser cladding and thermal spray processes on cast iron rotors to combat the corrosion issues. However, mentioned surface coating processes increase the cost of brake rotors and there is a need to search for cost-effective coating processes. In this research, a new Al2O3-Ni composite coating was proposed for preparation of a commercial cast iron brake rotor using plasma electrolytic aluminating (PEA) followed by electroless nickel plating (ENP) processes.