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Journal Article

Sampling of Non-Volatile Vehicle Exhaust Particles: A Simplified Guide

2012-04-16
2012-01-0443
Recently, a particle number (PN) limit was introduced in the European light-duty vehicles legislation. The legislation requires measurement of PN, and particulate mass (PM), from the full dilution tunnel with constant volume sampling (CVS). Furthermore, PN measurements will be introduced in the next stage of the European Heavy-Duty regulation. Heavy-duty engine certification can be done either from the CVS or from a partial flow dilution system (PFDS). For research and development purposes, though, measurements are often conducted from the raw exhaust, thereby avoiding the high installation costs of CVS and PFDS. Although for legislative measurements requirements exist regarding sampling and transport of the aerosol sample, such requirements do not necessarily apply for raw exhaust measurements. Thus, measurement differences are often observed depending on where in the experimental set up sampling occurs.
Journal Article

A New Approach for Very Low Particulate Mass Emissions Measurement

2013-04-08
2013-01-1557
Pending reductions in light duty vehicle PM emissions standards from 10 to 3 mg/mi and below will push the limits of the gravimetric measurement method. At these levels the PM mass collected approaches the mass of non-particle gaseous species that adsorb onto the filter from exhaust and ambient air. This introduces an intrinsic lower limit to filter based measurement that is independent of improvements achieved in weighing metrology. The statistical variability of back-up filter measurements at these levels makes them an ineffective means for correcting the adsorption artifact. The proposed subtraction of a facility based estimate of the artifact will partially alleviate the mass bias from adsorption, but its impact on weighing variability remains a problem that can reach a significant fraction of the upcoming 3 and future 1 mg/mi standards. This paper proposes an improved PM mass method that combines the gravimetric filter approach with real time aerosol measurement.
Technical Paper

Comparison of Particulate Matter and Number Emissions from a Floating and a Fixed Caliper Brake System of the Same Lining Formulation

2020-10-05
2020-01-1633
The particulate emissions of two brake systems were characterized in a dilution tunnel optimized for PM10 measurements. The larger of them employed a fixed caliper (FXC) and the smaller one a floating caliper (FLC). Both used ECE brake pads of the same lining formulation. Measured properties included gravimetric PM2.5 and PM10, Particle Number (PN) concentrations of both untreated and thermally treated (according to exhaust PN regulation) particles using Condensation Particle Counters (CPCs) having 23 and 10 nm cut-off sizes, and an Optical Particle Sizer (OPS). The brakes were tested over a section (trip-10) novel test cycle developed from the database of the Worldwide harmonized Light-Duty vehicles Test Procedure (WLTP). A series of trip-10 tests were performed starting from unconditioned pads, to characterize the evolution of emissions until their stabilization. Selected tests were also performed over a short version of the Los Angeles City Cycle.
Technical Paper

Measurement of Dry Soot and Particulate Matter from Two-Stroke and Four-Stroke Snowmobiles

2010-09-28
2010-32-0042
Recent increases in emissions regulations within the snowmobile industry have led to significant advancements in fuel, exhaust, and control systems on snowmobiles. However, particulate matter is currently an unregulated exhaust component of snowmobile engines. The measurement of dry soot as well as particulate matter from snowmobiles is the focus of this paper. Two industry-representative snowmobiles were chosen for this research which included a 2006 Yamaha Nytro carbureted four-stroke and a 2009 Ski-Doo MX-Z direct-injected two-stroke. Measurements for each snowmobile included gaseous emissions (CO₂, CO, NOx, O₂, and THC), particulate matter collected on quartz filters, and dry soot measured using an AVL Micro Soot Sensor. Each snowmobile was tested over the industry-standard five-mode emissions certification test cycle to determine the emissions, dry soot, and particulate matter levels from idle to wide open throttle (full-load).
Technical Paper

DVE - Direct Vehicle Exhaust Flow Measurement using Head-type Flowmeters

2003-03-03
2003-01-0782
When exhaust emissions from a vehicle are measured, a flow rate is needed in addition to pollutant concentrations in order to calculate the mass emitted. The highly unsteady flow from an internal combustion engine presents measurement challenges to exhaust flowmeters, especially at idle. Mass measurement methods used in the past have gotten around this problem by a variable dilution scheme (CVS) that measures a different, more favorable flow, but reduces and can contaminate exhaust gas concentration levels. The flow measurement system described here makes possible a more accurate measure of the vehicle exhaust flow by means of a number of design features. This improves considerably the cost effectiveness and accuracy of emissions measurement techniques such as the Bag-Minidiluter sampling system and raw modal analysis.
Technical Paper

Accuracy of Particle Number Measurements from Partial Flow Dilution Systems

2011-09-11
2011-24-0207
The measurement of the particle number (PN) concentration of non-volatile particles ≻23 nm was introduced in the light-duty vehicles regulation; the heavy-duty regulation followed. Based on the findings of the Particle Measurement Program (PMP), heavy-duty inter-laboratory exercise, the PN concentration measurement can be conducted either from the full dilution tunnel with constant volume sampling (CVS) or from the partial flow dilution system (PFDS). However, there are no other studies that investigate whether the PN results from the two systems are equivalent. In addition, even the PMP study never investigated the uncertainty that is introduced at the final result from the extraction of a flow by a PN system from the PFDS. In this work we investigate the uncertainty for the three possible cases, i.e., considering a constant extracted flow from the PFDS, sending a signal with 1 Hz frequency to the PFDS, or feeding back the extracted flow to the PFDS.
Technical Paper

CMS - An Evolution of the CVS - A Full Flow, Constant Mass Flow, Sampling System

2006-04-03
2006-01-1514
The CMS system commissioned by EPA and built by AVL, is a “start from a clean sheet of paper” approach to a full flow sampling system for aerosol matter from engine exhaust. The challenge of measuring 2007 level post DPF type particulate matter and polyaromatic hydrocarbons led to this re-thinking of sampler design. Previously used CVS designs had evolved to include elements that were not ideally suited for scaling up to large flow rates, and had mixing tunnels that were less than ideal for the sampling of complicated aerosols. The solution presented in this paper used ultrasonic time-of-flight flowmeters in place of the usual Venturi flow tubes, reducing the size and cost of air handling components. Acoustically designed dampeners were used to reduce pulsation disturbances to the flow measurement.
Technical Paper

Evaluation of Horiba MEXA 7000 Bag Bench Analyzers for Single Range Operation

1999-03-01
1999-01-0147
Dynamic single range analyzers are designed to cover the wide range of concentrations that once required multiple ranges. The use of single range analyzers is attractive because they can significantly reduce installation costs, gas cylinder charges, and facility storage space. The new technology relies on expansion of the digital dynamic range of the analyzer combined with the availability of a high accuracy gas divider with a 500 to one dilution ratio and a large number of cut points. A series of four MEXA 7000 series bag bench analyzers manufactured by Horiba Instruments, Inc., were evaluated to compare multiple range operation with single range operation. This report describes the operation of these analyzers and summarizes the evaluation methods and results. The evaluation verified the ability of the analyzers to operate in single range mode.
Technical Paper

Design of a Laboratory Sampling System for Brake Wear Particle Measurements

2022-09-19
2022-01-1179
Brake wear is one of the dominant sources of traffic-related particulate matter emissions and is associated with various adverse environmental and health hazards. To address this issue, the UNECE mandated the Particle Measurement Program to develop a harmonized methodology for sampling and measuring brake wear particles with a full-flow sampling tunnel on a brake dynamometer. Here we present the design of a novel, fully PMP compliant sampling tunnel. The dimensions and general layout of the tunnel are based on minimization of super-micron particle losses and consideration of space limitations in brake-dynamometer setups as well as the need for efficient utilization of the test facilities (reduced testing times). Numerical calculations suggested that the critical section of the system is the sampling train from the sample probes to the instrumentation inlet/filter holder.
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