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The latest legislation requires a dramatic reduction of motor vehicle exhaust emission. This is also a big challenge for emission measurement instrumentation, because of almost zero concentrations of certain components in the exhaust. For current measurement devices, which are recommended by the legislation, it is almost impossible to determine such low emission levels with adequate accuracy. The paper describes a new Constant Volume Sampling (CVS) system with reduced dilution, warming and quick flow rate changing capability. Possible solutions are discussed and the properties of data measured with test facilities which are prepared to cover S-ULEV and EURO IV applications are described. Also the selection of used materials is of rising importance. The tests were performed on a dynamic engine test bed which was equipped with such a CVS system and with emission analyzing systems for raw exhaust and diluted measurements.