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Technical Paper

The Fatigue Performance of High Temperature Vacuum Carburized Nb Modified 8620 Steel

2007-04-16
2007-01-1007
The bending fatigue performance of high temperature (1050 °C) vacuum carburized Nb modified 8620 steel, with niobium additions of 0.02, 0.06 and 0.1 wt pct, was evaluated utilizing a modified Brugger specimen geometry. Samples were heated at two different rates (20 and 114 °C min-1) to the carburizing temperature resulting in different prior austenite grain structures that depended on the specific Nb addition and heating rate employed. At the lower heating rate, uniform fine grained prior austenite grain structures developed in the 0.06 and 0.1 Nb steels while a duplex grain structure with the presence of large (>200 μm grains) developed in the 0.02 Nb steel. At the higher heating rate the propensity for abnormal grain growth was highest in the 0.02 Nb steel and complete suppression of abnormal grain growth was achieved only with the 0.1 Nb steel.
Technical Paper

The Effect of Reheat Treatments on Fatigue and Fracture of Carburized Steels

1994-03-01
940788
The effects of austenite grain size on the bending fatigue crack initiation and fatigue performance of gas carburized, modified 4320 steels were studied. The steels were identical in composition except for phosphorus concentration which ranged between 0.005 and 0.031 wt%. Following the carburizing cycle, specimens were subjected to single and triple reheat treatments of 820°C for 30 minutes to refine the austenite grain structure, and oil quenched and tempered at 150°C. Specimens subjected to bending fatigue were characterized by light metallography to determine microstructure and grain size, X-ray analysis for retained austenite and residual stress measurements, and scanning electron microscopy for examination of fatigue crack initiation and propagation. The surface austenite grain size ranged from 15 μm in the as-carburized condition to 6 and 4 μm diameter grain size for the single and triple reheat conditions, respectively.
Technical Paper

Response to Hydrogen Charging in High Strength Automotive Sheet Steel Products

2003-03-03
2003-01-0525
The influences of laboratory-induced hydrogen on the tensile deformation and fracture behavior of selected sheet steels including conventional DQSK and HSLA steels as well as newer DP and TRIP grades were evaluated. The effects of cold work, simulated paint baking, and natural aging were considered. Hydrogen effects were observable by increased flow stress, decreased ductility, altered neck geometry, and altered fracture mechanisms. Differences among the steels and conditions were observed and interpreted on the basis of microstructure, fracture behavior, and theories of hydrogen embrittlement.
Technical Paper

Optimized Carburized Steel Fatigue Performance as Assessed with Gear and Modified Brugger Fatigue Tests

2002-03-04
2002-01-1003
The effectiveness of three different techniques, designed to improve the bending fatigue life in comparison to conventionally processed gas-carburized 8620 steel, were evaluated with modified Brugger bending fatigue specimens and actual ring and pinion gears. The bending fatigue samples were machined from forged gear blanks from the same lot of material used for the pinion gear tests, and all processing of laboratory samples and gears was done together. Fatigue data were obtained on standard as-carburized parts and after three special processing histories: shot-peening to increase surface residual stresses; double heat treating to refined austenite grain size; and vacuum carburizing to minimize intergranular oxidation. Standard room-temperature S-N curves and endurance limits were obtained with the laboratory samples. The pinions were run as part of a complete gear set on a laboratory dynamometer and data were obtained at two imposed torque levels.
Technical Paper

Investigation of S-N Test Data Scatter of Carburized 4320 Steel

2007-04-16
2007-01-1006
A series of bending fatigue tests were conducted and S-N data were obtained for two groups of 4320 steel samples: (1) carburized, quenched and tempered, (2) carburized, quenched, tempered and shot peened. Shot peening improved the fatigue life and endurance limit. The S-N data exhibited large scatter, especially for carburized samples and at the high cycle life regime. Sample characterization work was performed and scatter bands were established for residual stress distributions, in addition to fracture and fatigue properties for 4320 steel. Moreover, a fatigue life analysis was performed using fracture mechanics and strain life fatigue theories. Scatter in S-N curves was established computationally by using the lower bound and upper bound in materials properties, residual stress and IGO depth in the input data. The results for fatigue life analysis, using either computational fracture mechanics or strain life theory, agreed reasonably well with the test data.
Technical Paper

Influence of Coating Microstructure on the Fatigue Properties of Zinc Coated Sheet Steels

1998-02-23
980955
The influence of coatings on fatigue behavior has been examined for the following commercially produced sheet steels: uncoated titanium stabilized interstitial-free (IF); electrogalvanized titanium stabilized IF; hot-dip galvanized aluminum killed, drawing quality (AKDQ); and galvannealed AKDQ. Fully reversed bending fatigue tests were conducted at ambient temperature on Krouse-type flexural fatigue machines. A dependence of crack development was observed and correlated to the microstructure and properties of the different coatings. Furthermore, a functional design relationship for each material was determined through stress-life analysis. The experimentally determined fatigue properties were compared to conventional estimates based on tensile properties which ignore coating effects. The results of this work suggest that ductile coatings may enhance fatigue resistance, while brittle coatings may reduce fatigue life.
Technical Paper

Hydrogen Embrittlement Susceptibility of Case Hardened Steel Fasteners

2018-04-03
2018-01-1240
This work establishes the relationship between core hardness, case hardness, and case depth on susceptibility to hydrogen embrittlement of case hardened steel fasteners. Such fasteners have a high surface hardness in order to create their own threads in a mating hole, and are commonly used to attach bracketry and sheet metal in automotive applications. While case hardened fasteners have been studied previously, there are currently no processing guidelines supported by quantitative data for fastener standards. Through sustained load embrittlement testing techniques, the susceptibility of case hardened steel tapping screws to internal and environmental hydrogen embrittlement is examined. Further characterization of the fastener samples through microhardness testing, microstructure review, and fracture surface examination allows the investigation of susceptibility thresholds. It is shown that core hardness is the primary consideration for susceptibility.
Technical Paper

Handheld Fine Water Mist Extinguisher for Spacecraft

2008-06-29
2008-01-2040
Fine water mist has become a commercial technology for fire suppression in multiple applications. With funding from NASA, ADA Technologies, Inc. (ADA) is developing a handheld fine water mist fire extinguisher for use on manned spacecraft and in future planetary habitats. This design employs only water and nitrogen as suppression agents to allow local refill and reuse. The prototype design incorporates features to generate a uniform fine water mist regardless of the direction of the gravitational vector or lack of gravity altogether. The system has been proven to extinguish open fires and hidden fire scenarios in tests conducted at the Colorado School of Mines (CSM). This design can be deployed as a portable extinguisher or as an automated system for local fire protection in instrument racks or storage spaces. Continued development will result in prototype hardware suitable for use on future manned spacecraft.
Technical Paper

Frictional Behavior of Electrogalvanized Sheet Steels

1993-03-01
930809
The frictional behavior of two nominally 70 g/m2 electrogalvanized sheet steels, mechanically processed with a series of surface roughnesses and coating morphologies, were evaluated with the bending under tension test. The crystallographic textures for the as-received materials were different; one was primarily prismatic with a friction coefficient of 0.14 and the other was primarily low angle pyramidal with a friction coefficient of 0.20. The friction coefficients were changed by surface modifications and values as high as 0.31 were observed. Friction data are discussed in terms of surface roughness, interfacial contact pressure, true contact area, and crystallographic texture. Results are interpreted on the basis of the deformation characteristics of the zinc coatings and with respect to overall sheet formability characteristics.
Journal Article

Expanding the Experimental Capabilities of the Ignition Quality Tester for Autoigniting Fuels

2010-04-12
2010-01-0741
This paper reports the development of new fuel ignition quality and combustion experiments performed using the Ignition Quality Tester (IQT). Prior SAE papers (961182, 971636, 1999-01-3591, and 2001-01-3527) documented the development of the IQT constant volume combustion chamber experimental apparatus to measure ignition qualities of diesel-type fuels. The ASTM International test method D6890 was developed around the IQT device to allow the rapid determination of derived cetane number (DCN). Interest in chemical kinetic models for the ignition of diesel and biodiesel model compounds is increasing to support the development of advanced engines and fuels. However, rigorous experimental validation of these kinetic models has been limited for a variety of reasons. Shock tubes and rapid compression machines are typically limited to premixed gas-phase studies, for example.
Technical Paper

European Lunar Base Concepts

2003-07-07
2003-01-2652
Propelled by the renewed international interest in returning to the Moon, an international consortium organized the first European Lunar Base Design Workshop in the summer of 2002. The objective of this Workshop was to propose new design concepts for human and robotic exploration of the Moon and move beyond the outdated ‘man-in-a-can’ genre of space architecture. The Workshop introduced a new genre in lunar base architecture, deriving from bold, innovative and unconventional thinking. It generated experimental concepts for sustainable, advanced, user-oriented architectures for future lunar bases. The Workshop participants chose diverse moon mission scenarios including ice mining, solar cell production, lunar telescopes, He3 mining, research and commercial operations. This paper will present the most important explorations and concepts from this Workshop. It will discuss the rationale behind adopting a multidisciplinary and multicultural design studio approach.
Technical Paper

Effects of Subzero Treatments on the Bending Fatigue Performance of Carburized SAE-4320 and SAE-9310 Steels

1996-02-01
960313
The effects of subzero treatments on the bending fatigue performance of carburized gear steels were investigated by cantilever bending fatigue testing. Specimens were machined from SAE-4320 and SAE-9310 bar stock steel, gas-carburized, quenched, tempered at 175°C, subzero cooled to -73°C and -196°C, and tempered at 175°C. Bending fatigue specimens were characterized by light metallography to determine microstructure and prior austenite grain size, x-ray diffraction for residual stress and retained austenite contents, microhardness testing, and scanning electron microscopy to evaluate fatigue crack initiation, propagation and overload. Refrigeration treatments caused additional transformation of retained austenite and increased surface hardness and compressive residual stresses. Bending fatigue endurance limits for the SAE-4320 specimens were determined to be 1310 MPa for the as-carburized condition, 1170 MPa for the -73°C condition, and 1280 MPa for the -196°C condition.
Journal Article

Effects of Chemical Composition, Heat Treatment, and Microstructure in Splittable Forged Steel Connecting Rods

2015-04-14
2015-01-0522
Fracture split forged steel connecting rods are utilized in many new high performance automotive engines to increase durability. Higher strength levels are needed as the power density increases. Fracture splitting without plastic deformation is necessary for manufacturability. Metallurgical design is a key for achieving the required performance levels. Several medium carbon steels containing 0.07 wt pct P, 0.06 wt pct S and various amounts of Mn, Si, V, and N were produced by vacuum induction melting laboratory heats and hot working the cast ingots into plates. The plates were cooled at varying rates to simulate typical cooling methods after forging. Microstructures were generally ferrite and pearlite as evaluated by light optical and scanning electron microscopy. Mechanical properties were determined by standard tensile tests, high strain rate notched tensile tests, and Charpy V-notch impact tests to assess “splittability”.
Technical Paper

Comparison of Single Gear Tooth and Cantilever Beam Bending Fatigue Testing of Carburized Steel

1995-02-01
950212
The bending fatigue performance of gears, cantilever beam specimens, and notched-axial specimens were evaluated and compared. Specimens were machined from a modified SAE-4118 steel, gas-carburized, direct-quenched and tempered. Bending fatigue specimens were characterized by light metallography to determine microstructure and prior austenite grain size, x-ray analysis for residual stress and retained austenite measurements, and scanning electron microscopy to evaluate fatigue crack initiation, propagation and overload. The case and core microstructures, prior austenite grain sizes and case hardness profiles from the various types of specimens were similar. Endurance limits were determined to be about 950 MPa for both the cantilever beam and notched-axial fatigue specimens, and 1310 MPa for the single gear tooth specimens.
Technical Paper

Combined Synchrotron X-Ray Diffraction and Digital Image Correlation Technique for Measurement of Austenite Transformation with Strain in TRIP-Assisted Steels

2016-04-05
2016-01-0419
The strain-induced diffusionless shear transformation of retained austenite to martensite during straining of transformation induced plasticity (TRIP) assisted steels increases strain hardening and delays necking and fracture leading to exceptional ductility and strength, which are attractive for automotive applications. A novel technique that provides the retained austenite volume fraction variation with strain with improved precision is presented. Digital images of the gauge section of tensile specimens were first recorded up to selected plastic strains with a stereo digital image correlation (DIC) system. The austenite volume fraction was measured by synchrotron X-ray diffraction from small squares cut from the gage section. Strain fields in the squares were then computed by localizing the strain measurement to the corresponding region of a given square during DIC post-processing of the images recorded during tensile testing.
Journal Article

Carbon and Manganese Effects on Quenching and Partitioning Response of CMnSi-Steels

2015-04-14
2015-01-0530
Quenching and partitioning (Q&P) is a novel heat treatment to produce third generation advanced high-strength steels (AHSS). The influence of carbon on mechanical properties of Q&P treated CMnSi-steels was studied using 0.3C-1.5Mn-1.5Si and 0.4C-1.5Mn-1.5Si alloys. Full austenitization followed by two-step Q&P treatments were conducted using varying partitioning times and a fixed partitioning temperature of 400 °C. The results were compared to literature data for 0.2C-1.6Mn-1.6Si, 0.2-3Mn-1.6Si and 0.3-3Mn-1.6Si Q&P treated steels. The comparison showed that increasing the carbon content from 0.2 to 0.4 wt pct increased the ultimate tensile strength by 140 MPa per 0.1 wt pct C up to 1611 MPa without significantly decreasing ductility for the partitioning conditions used. Increased alloy carbon content did not substantially increase the retained austenite fractions. The best combinations of ultimate tensile strength and total elongation were obtained using short partitioning times.
Technical Paper

Bending Fatigue Performance of Gas- and Plasma-Carburized Steels

1999-03-01
1999-01-0602
This study evaluated the bending fatigue performance of a modified SAE 4320 steel as a function of carburizing technique. S-N curves and endurance limits were established by fatigue testing modified Brugger-type specimens that are designed to simulate a single gear tooth. Fractured specimens were examined by light and electron microscopy to determine crack initiation sites, establish the extent of stable crack propagation, and analyze surface oxide types and distributions. Test results show that plasma-carburizing boosted the endurance limit of an oxidation-susceptible gear steel from 1100 MPa to 1375 MPa. Fatigue endurance limits in excess of 1400 MPa had previously been achieved in gas-carburized SAE 4320 steels by reheat treatments and reductions in high-oxidation potential elements. The level of improvement observed in this study suggests that any of these advanced processing techniques can allow significant size reductions and weight savings in automotive transmission gears.
Technical Paper

Bending Fatigue Performance of Carburized 4320 Steel

1993-03-01
930963
The bending fatigue performance of four heats of carburized, commercially-produced SAE 4320 steel was evaluated. Simulated gear tooth in bending (SGTB) cantilever beam specimens from each heat were identically carburized and fatigue tested in the direct quenched condition after carburizing. The microstructure and fracture surfaces of all specimens were characterized with light and electron microscopy. The four direct quenched sets of specimens performed similarly in low cycle fatigue. Endurance limits among the direct quenched specimens ranged between 1100 and 1170 MPa (160 and 170 ksi) and intergranular cracking dominated fatigue crack initiation. An additional set of specimens from one of the heats was reheated after carburizing. The fatigue performance of the reheated specimens was superior to that of the direct quenched specimens in both the low and high cycle regions. The effects of inclusion content, microstructure, and residual stresses on fatigue performance are discussed.
Journal Article

Bake Hardening Behavior of DP, TBF, and PHS Steels with Ultimate Tensile Strengths Exceeding 1 GPa

2020-04-14
2020-01-0536
Third generation advanced high strength steels (AHSS) have been developed combining high strength and formability, allowing for lightweighting of vehicle structural components. These AHSS components are exposed to paint baking operations ranging in time and temperature to cure the applied paint. The paint baking treatment, combined with straining induced from part forming, may lead to increased in-service component performance due to a strengthening mechanism known as bake hardening. This study aims to quantify the bake hardening behavior of select AHSS grades. Materials investigated were press hardenable steels (PHS) 1500 and 2000; transformation induced plasticity (TRIP) aided bainitic ferrite (TBF) 1000 and 1200; and dual phase (DP) 1000. The number designations of these grades refer to minimum as-received ultimate tensile strengths in MPa. Paint baking was simulated using industrially relevant times and temperatures from 15 to 60 min and 120 to 200 °C, respectively.
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