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The bending fatigue performance of high temperature (1050 °C) vacuum carburized Nb modified 8620 steel, with niobium additions of 0.02, 0.06 and 0.1 wt pct, was evaluated utilizing a modified Brugger specimen geometry. Samples were heated at two different rates (20 and 114 °C min-1) to the carburizing temperature resulting in different prior austenite grain structures that depended on the specific Nb addition and heating rate employed. At the lower heating rate, uniform fine grained prior austenite grain structures developed in the 0.06 and 0.1 Nb steels while a duplex grain structure with the presence of large (>200 μm grains) developed in the 0.02 Nb steel. At the higher heating rate the propensity for abnormal grain growth was highest in the 0.02 Nb steel and complete suppression of abnormal grain growth was achieved only with the 0.1 Nb steel.

High strain rate sheet tensile tests (up to 300s-1) and Ohio State University (OSU) formability tests (up to an estimated strain rate of 10s-1) were performed to examine the effect of strain rate on the mechanical properties and formability of five ferritic stainless steels: HIGH PERFORMANCE-10™ 409 (HP-10 409), ULTRA FORM® 409 (UF 409), HIGH PERFORMANCE-10™ 439 (HP-10 439), two thicknesses of 18 Cr-Cb™ stainless steel, all supplied by AK Steel, and Duracorr®, a ferrite-tempered martensite dual-phase stainless steel supplied by Bethlehem Steel Corporation. Tensile results show that increasing strain rate resulted in increases in yield stress, flow stress, and stress at instability for all alloys tested. In addition, increases in uniform and total elongation were also found for each of the five alloys.

With the increased use of tubular steel products, especially for automotive hydroforming applications, there is increased interest in understanding the mechanical properties measured by tensile tests from specimens of different orientations in the tube. In this study, two orientations of tensile specimens were evaluated -- axial specimens with and without flattening and flattened circumferential specimens. Three steels were evaluated -- two thicknesses of aluminum killed drawing quality (AKDQ) steel and one thickness of high strength low alloy (HSLA) steel. Mechanical property data were obtained from the flat stock, conventional production tubes and quasi tubes. Quasi tubes were produced from the flat stock on a 3-roll bender, but the quasi tube was not welded or sized.

Drawbeads in production stamping dies often have insufficient penetration of the male bead into the female cavity. With insufficient penetration, the actual bending radii of the sheet metal are larger than the geometrical radii of the drawbead. The actual bending radii in the sheet directly affect the force that restrains sheet movement. To predict the restraining stress due to a drawbead, it is necessary to know the actual bending radii in the sheet as it passes though the drawbead. Data from a previous study are used to develop empirical regression equations for predicting measured radii of the sheet that is bent around the radii in a drawbead. A physical model for the evolution of the sheet radii as the drawbead closes is proposed. This model is consistent with the empirical equations and the mechanics of the sheet bending process.

The effectiveness of three different techniques, designed to improve the bending fatigue life in comparison to conventionally processed gas-carburized 8620 steel, were evaluated with modified Brugger bending fatigue specimens and actual ring and pinion gears. The bending fatigue samples were machined from forged gear blanks from the same lot of material used for the pinion gear tests, and all processing of laboratory samples and gears was done together. Fatigue data were obtained on standard as-carburized parts and after three special processing histories: shot-peening to increase surface residual stresses; double heat treating to refined austenite grain size; and vacuum carburizing to minimize intergranular oxidation. Standard room-temperature S-N curves and endurance limits were obtained with the laboratory samples. The pinions were run as part of a complete gear set on a laboratory dynamometer and data were obtained at two imposed torque levels.

An iterative learning control (ILC) algorithm has been developed for a test cell electro-hydraulic, fully flexible valve actuation system to track valve lift profile under steady-state and transient operation. A dynamic model of the plant was obtained from experimental data to design and verify the ILC algorithm. The ILC is implemented in a prototype controller. The learned control input for two different lift profiles can be used for engine transient tests. Simulation and bench test are conducted to verify the effectiveness and robustness of this approach. The simple structure of the ILC in implementation and low cost in computation are other crucial factors to recommend the ILC. It does not totally depend on the system model during the design procedure. Therefore, it has relatively higher robustness to perturbation and modeling errors than other control methods for repetitive tasks.

A series of bending fatigue tests were conducted and S-N data were obtained for two groups of 4320 steel samples: (1) carburized, quenched and tempered, (2) carburized, quenched, tempered and shot peened. Shot peening improved the fatigue life and endurance limit. The S-N data exhibited large scatter, especially for carburized samples and at the high cycle life regime. Sample characterization work was performed and scatter bands were established for residual stress distributions, in addition to fracture and fatigue properties for 4320 steel. Moreover, a fatigue life analysis was performed using fracture mechanics and strain life fatigue theories. Scatter in S-N curves was established computationally by using the lower bound and upper bound in materials properties, residual stress and IGO depth in the input data. The results for fatigue life analysis, using either computational fracture mechanics or strain life theory, agreed reasonably well with the test data.

This work establishes the relationship between core hardness, case hardness, and case depth on susceptibility to hydrogen embrittlement of case hardened steel fasteners. Such fasteners have a high surface hardness in order to create their own threads in a mating hole, and are commonly used to attach bracketry and sheet metal in automotive applications. While case hardened fasteners have been studied previously, there are currently no processing guidelines supported by quantitative data for fastener standards. Through sustained load embrittlement testing techniques, the susceptibility of case hardened steel tapping screws to internal and environmental hydrogen embrittlement is examined. Further characterization of the fastener samples through microhardness testing, microstructure review, and fracture surface examination allows the investigation of susceptibility thresholds. It is shown that core hardness is the primary consideration for susceptibility.

Fine water mist has become a commercial technology for fire suppression in multiple applications. With funding from NASA, ADA Technologies, Inc. (ADA) is developing a handheld fine water mist fire extinguisher for use on manned spacecraft and in future planetary habitats. This design employs only water and nitrogen as suppression agents to allow local refill and reuse. The prototype design incorporates features to generate a uniform fine water mist regardless of the direction of the gravitational vector or lack of gravity altogether. The system has been proven to extinguish open fires and hidden fire scenarios in tests conducted at the Colorado School of Mines (CSM). This design can be deployed as a portable extinguisher or as an automated system for local fire protection in instrument racks or storage spaces. Continued development will result in prototype hardware suitable for use on future manned spacecraft.

Punch-stretch tests to determine formability of type 304 stainless steel sheet were conducted using a hemispherical dome test. Sheets of 19.1 mm width and 177.8 mm width were stretched on a 101.6 mm diameter punch at punch rates between 0.042 to 2.12 mm/sec with three lubricant systems: a mineral seal oil, thin polytetrafluoroethelyne sheet with mineral seal oil, and silicone rubber with mineral seal oil. The resulting strain distributions were measured and the amount of martensite was determined by magnetic means. Increasing lubricity resulted in more uniform strain distributions while increased punch rates tended to decrease both strain and transformation distributions. High forming limit values were related to the formation of high and uniformly distributed martensite volume fractions during deformation. The results of this study are interpreted with an analysis of the effects of strain and temperature on strain induced martensite formation in metastable austenitic stainless steels.

The effects of several variables on pitting fatigue life of carburized steels were analyzed using a geared roller test machine (GRTM). The material variables that were primarily used to influence retained austenite include aim surface carbon concentration (0.8 % and 0.95 %), alloy (SAE 4320 and a modified SAE 4122), and cold treatment (performed on one material condition per alloy). Testing variables included contact stress in addition to a variation in lambda ratio (oil film thickness/surface roughness), arising from variation in roughness among the machined surfaces. Test results are presented, and differences in performance are considered in terms of material and testing variables. A primary observation from these results is an improvement in contact fatigue resistance apparently arising from cold-treatment and the associated reduction of retained austenite at the surface.

The effects of elevated testing temperature on the fatigue behavior of carburized steel were evaluated by testing modified Brügger bending fatigue specimens at room temperature, 90 °C and 150 °C. SAE 4023, SAE 4320, and SAE 9310 steel were studied to assess the influence of alloy content and stability of retained austenite. Fatigue samples were gas-carburized and tested in air at 30 Hz with a stress ratio of 0.1. An infrared spot lamp was used to heat samples to 90 °C (150 °F) or 150 °C (302 °F) during testing. S-N curves were developed for the room temperature baseline tests as well as elevated temperature tests. The endurance limits determined are as follows: SAE 4023-RT (1170 MPa), SAE 4023-90°C (1140 MPa), SAE 4320-RT (1210 MPa), SAE 4320-90°C (1280 MPa), SAE 9310-RT (1380 MPa), SAE 9310-90°C (1240 MPa).

This project investigated the effect of carburizing carbon-potential and thermal history on the bending fatigue performance of carburized SAE 4320 gear steel. Modified-Brugger cantilever bending fatigue specimens were carburized at carbon potentials of 0.60, 0.85, 1.05, and 1.25 wt. pct. carbon, and were either quenched and tempered or quenched, tempered, reheated, quenched, and tempered. The reheat treatment was designed to lower the solute carbon content in the case through the formation of transition carbides and refine the prior austenite grain size. Specimens were fatigue tested in a tension/tension cycle with a minimum to maximum stress ratio of 0.1. The bending fatigue results were correlated with case and core microstructures, hardness profiles, residual stress profiles, retained austenite profiles, and component distortion.

The bending fatigue performance of gears, cantilever beam specimens, and notched-axial specimens were evaluated and compared. Specimens were machined from a modified SAE-4118 steel, gas-carburized, direct-quenched and tempered. Bending fatigue specimens were characterized by light metallography to determine microstructure and prior austenite grain size, x-ray analysis for residual stress and retained austenite measurements, and scanning electron microscopy to evaluate fatigue crack initiation, propagation and overload. The case and core microstructures, prior austenite grain sizes and case hardness profiles from the various types of specimens were similar. Endurance limits were determined to be about 950 MPa for both the cantilever beam and notched-axial fatigue specimens, and 1310 MPa for the single gear tooth specimens.

Quenching and partitioning (Q&P) is a novel heat treatment to produce third generation advanced high-strength steels (AHSS). The influence of carbon on mechanical properties of Q&P treated CMnSi-steels was studied using 0.3C-1.5Mn-1.5Si and 0.4C-1.5Mn-1.5Si alloys. Full austenitization followed by two-step Q&P treatments were conducted using varying partitioning times and a fixed partitioning temperature of 400 °C. The results were compared to literature data for 0.2C-1.6Mn-1.6Si, 0.2-3Mn-1.6Si and 0.3-3Mn-1.6Si Q&P treated steels. The comparison showed that increasing the carbon content from 0.2 to 0.4 wt pct increased the ultimate tensile strength by 140 MPa per 0.1 wt pct C up to 1611 MPa without significantly decreasing ductility for the partitioning conditions used. Increased alloy carbon content did not substantially increase the retained austenite fractions. The best combinations of ultimate tensile strength and total elongation were obtained using short partitioning times.

This study evaluated the bending fatigue performance of a modified SAE 4320 steel as a function of carburizing technique. S-N curves and endurance limits were established by fatigue testing modified Brugger-type specimens that are designed to simulate a single gear tooth. Fractured specimens were examined by light and electron microscopy to determine crack initiation sites, establish the extent of stable crack propagation, and analyze surface oxide types and distributions. Test results show that plasma-carburizing boosted the endurance limit of an oxidation-susceptible gear steel from 1100 MPa to 1375 MPa. Fatigue endurance limits in excess of 1400 MPa had previously been achieved in gas-carburized SAE 4320 steels by reheat treatments and reductions in high-oxidation potential elements. The level of improvement observed in this study suggests that any of these advanced processing techniques can allow significant size reductions and weight savings in automotive transmission gears.

To address the growing need for detailed chemistry in engine simulations, new software tools and validated data sets are being developed under an industry-funded consortium involving members from the automotive and fuels industry. The results described here include systematic comparison and validation of detailed chemistry models using a wide range of fundamental experimental data, and the development of software tools that support the use of detailed mechanisms in engineering simulations. Such tools include the automated reduction of reaction mechanisms for targeted simulation conditions. Selected results are presented and discussed.

ADA Technologies, Inc. has designed and built a microgravity-tolerant portable fire extinguisher prototype for use in manned spacecraft and planetary habitats. This device employs Fine Water Mist (FWM) as the fire extinguishing agent, and is refillable from standard stores on long-duration missions. The design uses a single storage tank for minimal mass and volume. The prototype employs a dual-fluid atomizer concept where the pressurant gas (nitrogen) also enhances the water atomization process to generate a droplet size distribution in the optimum diameter range of 10 to 50 micrometers. The expanding discharge gas plume carries the mist to the immediate vicinity of the fire where its extensive surface area promotes high heat transfer rates. A series of 80 fire suppression tests was recently completed to evaluate design options for the hardware and validate performance on three representative fire scenarios.

Direct osmotic concentration (DOC) is an integrated membrane treatment process designed for the reclamation of spacecraft wastewater. The system includes forward osmosis (FO), membrane evaporation, reverse osmosis (RO) and an aqueous phase catalytic oxidation (APCO) post-treatment unit. This document describes progress in the third year of a four year project to advance hardware maturity of this technology to a level appropriate for human rated testing. The current status of construction and testing of the final deliverable is covered and preliminary calculations of equivalent system mass are funished.