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Technical Paper

Understanding Soot Mediated Oil Thickening: Rotational Rheology Techniques to Determine Viscosity and Soot Structure in Peugeot XUD-11 BTE Drain Oils

2001-05-07
2001-01-1967
The Association des Constructeurs Européen d'Automobiles (ACEA) light duty diesel engine specifications requires a kinematic viscosity measurement technique for Peugeot XUD-11 BTE drain oils. This viscosity measurement is used to define the medium temperature dispersivity of soot in the drain oil.(1) This paper discusses the use of rotational rheology methods to measure the Newtonian character of XUD-11 drain oils. The calculation of the rate index using the Hershel Bulkley model indicates the level of non-Newtonian behavior of the drain oil and directly reflects the level of soot dispersion or agglomeration. This study shows that the more non-Newtonian the drain oil the greater the difference between kinematic and rotational viscosity measurements Oscillation (dynamic) rheological techniques are used to characterize build up of soot structure.
Technical Paper

Understanding Soot Mediated Oil Thickening Part 6: Base Oil Effects

1998-10-19
982665
One of the key functions of lubricating oil additives in diesel engines is to control oil thickening caused by soot accumulation. Over the last several years, it has become apparent that the composition of the base oil used within the lubricant plays an extremely important role in the oil thickening phenomenon. In particular, oil thickening observed in the Mack T-8 test is significantly affected by the aromatic content of the base oil. We have found that the Mack T-8 thickening phenomenon is associated with high electrical activity, i.e., engine drain oils which exhibit high levels of viscosity increase show significantly higher conductivities. These findings suggest that electrical interactions are involved in soot-induced oil thickening.
Technical Paper

The Use of Life Cycle Assessment with Crankcase Lubricants to Yield Maximum Environmental Benefit – Case Study of Residual Chlorine in Lubricant

2008-10-06
2008-01-2376
Life Cycle Assessment (LCA) is a methodology used to determine quantitatively the environmental impacts of a range of options. The environmental community has used LCA to study all of the impacts of a product over its life cycle. This analysis can help to prevent instances where a greater degree of environmental harm results when changes are made to products based on consideration of impacts in only part of the life cycle. This study applies the methodology to engine lubricants, and in particular chlorine limits in engine lubricant specifications. Concern that chlorine in lubricants might contribute to emissions from vehicle exhausts of polychlorinated dibenzo-p-dioxins (PCDD) and polychlorinated dibenzofurans (PCDF), collectively called PCDD/F, led to the introduction of chlorine limits in lubricant specifications. No direct evidence was available linking chlorine in lubricants to PCDD/F formation, but precautionary principles were used to set lubricant chlorine limits.
Technical Paper

The KA24E Engine Test for ILSAC GF-3 Part 1: Engine Design, Operating Conditions and Wear Mechanisms

1998-10-19
982625
The Nissan KA24E engine test is designated to replace the Ford Sequence VE engine test as the low temperature valve train wear requirement for ILSAC (International Lubricant Standardization and Approval Committee) GF-3. The KA24E (recently designated the Sequence IV A) represents much of the current world-wide material and design technology while retaining the sliding cam/follower contact found in earlier engine designs. The work presented here is the first of two reports. In this first report, the physical and chemical environment the KA24E engine presents a lubricant is characterized and compared to those of the Sequence VE engine. Valve train materials and wear modes are investigated and described. Although chemical analysis of drain oils indicate the KA24E procedure does not degrade the lubricant to the extent seen in the Sequence VE test, valve train wear appears to proceed in a similar manner in both tests.
Technical Paper

The Development of CVT Fluids with Higher Friction Coefficients

2003-05-19
2003-01-1978
The development of new transmission designs continues to affect the vehicle market. Continuously variable transmissions (CVTs) remain one of the more recent designs that impact the vehicle market. A desire for high belt-pulley capacity has driven studies concentrating on metal-on-metal (M/M) friction as a function of the CVT fluid. This paper describes the statistical techniques used to optimize the fluid friction as a function of additive components in a bench-scale, three-element test rig.
Technical Paper

Supporting the Transportation Industry: Creating the GC-LB and High-Performance Multiuse (HPM) Grease Certification Programs

2023-10-31
2023-01-1652
This paper outlines the history and background of the NLGI (formerly known as the National Lubricating Grease Institute) lubricating grease specifications, GC-LB classification of Automotive Service Greases as well as details on the development of new requirements for their High-Performance Multiuse (HPM) grease certification program. The performance of commercial lubricating grease formulations through NLGI's Certification Mark using the GC-LB Classification system and the recently introduced HPM grease certification program will be discussed. These certification programs have provided an internationally recognized specification for lubricating grease and automotive manufacturers, users and consumers since 1989. Although originally conceived as a specification for greases for the re-lubrication of automotive chassis and wheel bearings, GC-LB is today recognized as a mark of quality for a variety of different applications.
Technical Paper

Soot-Related Viscosity Increase - Further Studies Comparing the Mack T-11 Engine Test to Field Performance

2005-10-24
2005-01-3714
SAE 2004-01-3009 reported on work conducted to investigate the correlation between the Mack T-11 laboratory engine tests and vehicle field tests. It concluded that the T-11 test provides an effective screening tool to investigate soot-related viscosity increase, and the severity of the engine test limits provides a substantial margin of safety compared to the field. This follow-up paper continues the studies on the 2003 Mack CV713 granite dump truck equipped with an AI-427 internal EGR engine and introduces experimentation on a 2003 CX613 tractor unit equipped with an AC-460P cooled EGR engine. The paper further assesses the correlation of the field trials to the Mack T-11 engine test and reviews the impact of ultra low sulfur diesel (ULSD) and prototype CJ-4 lubricant formulations in these engines.
Technical Paper

Soot Related Viscosity Increase - A Comparison of the Mack T-11 Engine Test to Field Performance

2004-10-25
2004-01-3009
Soot related viscosity increase has been reported as a field issue in some diesel engines and this led to the development of the T-11 engine test, incorporated in the Mack EO-N Premium Plus 03 specification (014 GS 12037). This study compares T-11 laboratory engine tests and vehicle field tests and seeks to confirm the correlation between them. The findings are that the T-11 test provides an effective screening tool to investigate soot related viscosity increase, and the severity of the engine test limits gives a substantial margin of safety compared to the field. A complementary study was conducted in conjunction with this work that focuses on the successful application of electrochemical sensor technology to diagnose soot content and soot related viscosity increase. This will be the subject of a separate paper.
Technical Paper

Review of Exhaust Emissions of Compression Ignition Engines Operating on E Diesel Fuel Blends

2003-10-27
2003-01-3283
Recently, research and testing of oxygenated diesel fuels has increased, particularly in the area of exhaust emissions. Included among the oxygenated diesel fuels are blends of diesel fuel with ethanol, or E diesel fuels. Exhaust emissions testing of E diesel fuel has been conducted by a variety of test laboratories under various conditions of engine type and operating conditions. This work reviews the existing public data from previous exhaust emissions testing on E diesel fuel and includes new testing performed in engines of varied design. Emissions data compares E diesel fuel with normal diesel fuel under conditions of different engine speeds, different engine loads and different engine designs. Variations in performance under these various conditions are observed and discussed with some potential explanations suggested.
Technical Paper

Results of North American Field Trials Using Diesel Filters with a Copper Additive for Regeneration

1994-03-01
940455
SAE Paper 930131 outlined initial work performed on a diesel particulate filter system using a copper additive for regeneration. Laboratory evaluations of soot oxidation, fuel stability, and emissions reductions were presented along with preliminary field data. Since then, a total of thirty-four buses have been included in the North American fleet trials. The buses are powered by different engines and engine configurations. Results of the field trial are presented along with problems encountered and their resolution.
Technical Paper

Reducing Deposits in a DISI Engine

2002-10-21
2002-01-2660
Direct injection spark ignition (DISI) engine technology offers tremendous potential advantages in fuel savings and is likely to command a progressively increasing share of the European passenger vehicle market in the future. A concern is its propensity to form deposits on the inlet valve. In extreme cases, these deposits can lead to poor drivability and deteriorating emission performance. This inlet valve deposit build up is a well-known phenomenon in DISI engines since even additised fuel cannot wash over the back of intake valves to keep them clean. Two lubricants and two fuels were tested in a four car matrix. One of the lubricants was a fluid specifically developed by Lubrizol for DISI technology; the other was a baseline oil meeting Ford lubricants requirements and was qualified to ACEA A1/B1/ ILSAC GF2 performance level. Similarly, a baseline fuel was tested against an additised system.
Technical Paper

Over a Decade of LTMS

2004-06-08
2004-01-1891
The Lubricant Test Monitoring System (LTMS) is the calibration system methodology and protocol for North American engine oil and gear oil tests. This system, administered by the American Society for Testing Materials (ASTM) Test Monitoring Center (TMC) since 1992, has grown in scope from five gasoline engine tests to over two dozen gasoline, heavy duty diesel and gear oil tests ranging from several thousand dollars per test to almost one-hundred thousand dollars per test. LTMS utilizes Shewhart and Exponentially Weighted Moving Average (EWMA) control charts of reference oil data to assist in the decision making process on the calibration status of test stands and test laboratories. Equipment calibration is the backbone step necessary in the unbiased evaluation of candidate oils for oil quality specifications.
Technical Paper

Opportunity for Diesel Emission Reductions Using Advanced Catalysts and Water Blend Fuel

2000-03-06
2000-01-0182
This paper features the results of emission tests conducted on diesel oxidation catalysts, and the combination of diesel oxidation catalysts and water blend fuel (diesel fuel continuous emulsion). Vehicle chassis emission tests were conducted using an urban bus. The paper reviews the impact and potential benefits of combining catalyst and water blend diesel fuel technologies to reduce exhaust emissions from diesel engines.
Technical Paper

On-Board Sensor Systems to Diagnose Condition of Diesel Engine Lubricants - Focus on Soot

2004-10-25
2004-01-3010
Soot is a typical byproduct of the diesel fuel combustion process, and a portion of the soot inevitably enters an engine's crankcase. A key functionality of a diesel engine lubricant is to disperse and suspend soot so that larger-particle agglomerations are prevented. The role of soot agglomeration in abrasive engine wear and lubricant viscosity increase is the subject of a continuing investigation; however, what is generally known is that once an engine lubricant loses its ability to control soot and a rapid viscosity increase begins, the lubricant has reached the end of its useful life and should be changed to maximize engine performance and life. This issue of soot related viscosity increase is of such importance that the Mack T-11 engine test was developed as a laboratory tool to evaluate lubricants. The newly proposed Mack EO-N Premium Plus - 03 specification includes a T-11 performance requirement.
Technical Paper

Next Generation Torque Control Fluid Technology, Part IV: Using a New Split-μ Simulation Test for Optimizing Friction Material-Lubricant Hardware Systems

2010-10-25
2010-01-2230
Wet clutch friction devices are the primary means by which torque is transmitted through many of today's modern vehicle drivelines. These devices are used in automatic transmissions, torque vectoring devices, active on-demand vehicle stability systems and torque biasing differentials. As discussed in a previous SAE paper ( 2006-01-3271 - Next Generation Torque Control Fluid Technology, Part II: Split-Mu Screen Test Development) a testing tool was developed to correlate to full-vehicle split-mu testing for limited slip differential applications using a low speed SAE #2 friction test rig. The SAE #2 Split-Mu Simulation is a full clutch pack component level friction test. The purpose of this test is to allow optimization of the friction material-lubricant hardware system in order to deliver consistent friction performance over the life of the vehicle.
Technical Paper

Next Generation Torque Control Fluid Technology, Part III: Using an Improved Break-Away Friction Screen Test to Investigate Fundamental Friction Material-Lubricant Interactions

2010-10-25
2010-01-2231
Wet clutch friction devices are the primary means by which torque is transmitted in many of today's modern vehicle drivelines. These devices are used in automatic transmissions, torque vectoring devices, active on-demand vehicle stability systems, and torque biasing differentials. As discussed in a previous SAE paper ( 2006-01-3270 - Next Generation Torque Control Fluid Technology, Part I: Break-Away Friction Slip Screen Test Development), a testing tool was developed to simulate a limited slip differential break-away event using a Full Scale-Low Velocity Friction Apparatus (FS-LVFA). The purpose of this test was to investigate the fundamental interactions between lubricants and friction materials. The original break-away friction screen test, which used actual vehicle clutch plates and a single friction surface, proved a useful tool in screening new friction modifier technology.
Technical Paper

Next Generation Torque Control Fluid Technology, Part II: Split-Mu Screening Test Development

2006-10-16
2006-01-3271
The popularity of SUVs and light trucks in North America, combined with the return to rear-wheel-drive cars globally, is significantly increasing the installation of torque control devices that improve vehicle stability and drivability. As with other driveline hardware, it is important to optimize the friction material-lubricant-hardware system to ensure that a torque control device provides consistent performance over the life of the vehicle. While there are many publications on friction tests relevant to automatic transmission fluids, the literature relating to torque control testing is not as well developed. In this paper, we will describe a split-mu vehicle test and the development of a split-mu screening test. The screening test uses the SAE#2 friction test rig and shows how results from this test align with those from actual vehicle testing.
Technical Paper

Next Generation Torque Control Fluid Technology, Part I: Break-Away Friction Screening Test Development

2006-10-16
2006-01-3270
The popularity of SUVs and light trucks in North America, combined with the return to rear-wheel-drive cars globally, is significantly increasing the installation rates of torque control devices that improve vehicle stability and drivability. As with other driveline hardware, it is important to optimize the friction material-lubricant-hardware system in order to ensure that a torque control device provides consistent performance over the life of the vehicle. While there are many publications on friction tests relevant to automatic transmission fluids, the literature relating to torque control testing is not as well developed. In this paper we will describe the development of a break-away friction screening test using a Full-Scale Low-Velocity Friction Apparatus (FS-LVFA). Additionally, we will illustrate how this screening test can be used to investigate the fundamental friction material-lubricant interactions that occur in continuously engaged limited slip differentials.
Technical Paper

Mechanical Degradation of Viscosity Modifiers in Heavy Duty Diesel Engine Lubricants in Field Service

2003-10-27
2003-01-3223
Modern multi-grade engine lubricants are formulated to “stay in grade” during field service. Viscosity loss during the early stages of lubricant life is commonly believed to be caused by mechanical degradation of the viscosity modifier in the engine [1]. The Kurt Orbahn shear stability bench test (ASTM D 6278, 30 cycles) has been the industry standard predictor of viscosity loss due to polymer shear in heavy duty diesel engine lubricants. However, the Engine Manufacturers' Association (EMA) has expressed some concern that it underestimates the degree of polymer shear found in certain engines in the field, such as the Navistar 6.0L HEUI (Hydraulic Electronic Unit Injector) Power Stroke engine; a more severe bench test would serve to improve correlation with this and other similar engine designs. This paper offers a new approach for critically examining the relationship between the bench test and field performance.
Technical Paper

Lubricant Requirements of an Advanced Designed High Performance, Fuel Efficient Low Emissions V-6 Engine

2001-05-07
2001-01-1899
Modern high power density gasoline fueled engines place an ever-increasing demand on the engine lubricant. In this study, it is shown that advances in engine design to increase performance, improve fuel economy and lower emissions have outpaced the development of typical commercial engine lubricants. Advanced designed engines began to experience oil starvation as a result of a combination of driving cycles, oil quality and poor maintenance practices. The cause was traced to excessive increases in borderline pumping viscosity as measured by MRV TP-1 (ASTM D4684). Used oil analysis for MRV TP-1 showed viscosity greatly increased in excess of stay-in-grade requirements and in many cases the crankcase lubricant was solid at the temperature appropriate for its viscosity grade. However, at the same time CCS values were in grade or only slightly (1W grade) elevated.
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