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New combustion concepts developed in internal combustion engines such as homogeneous charge compression ignition (HCCI) have attracted serious attention due to the possibilities to simultaneously achieve higher efficiency and lower emissions, which will impact the environment positively. The HCCI combustion concept has potential of ultra-low NOX and particulate matter (PM) emission in comparison to a conventional gasoline or a diesel engine. Environmental Legislation Agencies are becoming increasingly concerned with particulate emissions from engines because the health and environmental effects of particulates emitted are now known and can be measured by sophisticated instruments. Particulate emissions from HCCI engines have been usually considered negligible, and the measurement of mass emission of PM from HCCI combustion systems shows their negligible contribution to PM mass. However some recent studies suggest that PM emissions from HCCI engines cannot be neglected.