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Non-Asbestos Organic (NAO) brake- material research has been significant in the last decade in an attempt to replace the conventional semi-metallic and asbestos based materials. Influence of ingredients in this multi-ingredient (generally 10-25 in different proportions) system on performance properties, however, is still not thoroughly researched area because of complexity involved and needs intensive efforts to understand this aspect. Graphite is one of the most important and almost inevitable ingredients in friction materials. A wide variety of graphite varying in origin, particle size, crystallinity, thermal conductivity etc. is used by the industry. An in-depth and systematic study on the influence of size of graphite on tribo-performance, however, is not available.

Phenolics or their modified versions are invariably used as binder materials for friction composites which consist of multiple ingredients. However, phenolics are known for their inherent serious problems such as; poor shelf life, which poses constraints for storage and transportation; evolution of harmful volatiles leading to voids, cracks and environmental pollution etc. In order to overcome these, three new thermoset able resins having oxazine ring were synthesized in the laboratory. These resins proved to be free from the above mentioned drawbacks. These were tribo-evaluated to explore the possibility of replacing currently used phenolics in friction materials. In order to evaluate their tribo-potential as friction materials, friction formulations (non-asbestos organic NAO) based on these resins were developed in the laboratory in the form of brake-pads and tensile specimens.