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The cycle-to-cycle variability and potential sources of unburned hydrocarbon (UHC) emissions are examined in a single-cylinder, light-duty diesel test engine operating in low-temperature combustion regimes. A fast flame ionization detector (FID) was employed to examine both cycle-to-cycle variations in UHC emissions and intra-cycle emissions behavior. A standard suite of emissions measurements, including CO, CO2, NOx, and soot, was also obtained. Measurements were made spanning a broad range of intake O2 concentrations-to examine the UHC behavior of dilution-controlled combustion regimes-and spanning a broad range of injection timings-to clarify the behavior of increased UHC emissions in late-injection combustion regimes. Both low- and moderate-loads were investigated. The cycle-resolved UHC data showed that the coefficient of variation of single-cycle UHC did not increase with increases in UHC emissions as either O2 concentration or injection timing was varied.