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Thermally Stratified Compressions Ignition (TSCI) is a new advanced, low temperature combustion concept that aims to control the thermal stratification in the cylinder in order to control the heat release process in a lean, compression-ignition combustion mode. This work uses “wet ethanol”, a mixture of 80% ethanol and 20% water by mass, to increase thermal stratification beyond what naturally occurs, via evaporative cooling of a split direct injection. TSCI with wet ethanol has previously shown the potential to increase the high-load limit when compared to HCCI. The experiments conducted in this paper aim to fundamentally understand the effect that injection strategy has on the heat release process in TSCI. TSCI employs a split-injection strategy in which an injection during the intake stroke allows the majority of the fuel to premix with the air and an injection during the compression stroke introduces the desired level of thermal stratification to control the heat release rate.