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Diesel engine ash emissions are composed of the non-combustible portions of diesel particulate matter derived mainly from lube oil, and over time can degrade diesel particulate filter performance. This paper presents results from a high temperature oxidation method (HTOM) used to estimate ash emissions, and engine oil consumption in real-time. Atomized lubrication oil and diesel engine exhaust were used to evaluate the HTOM performance. Atomized fresh and used lube oil experiments showed that the HTOM reached stable particle size distributions and concentrations at temperatures above 700°C. The HTOM produced very similar number and volume weighted particle size distributions for both types of lube oils. The particle number size distribution was unimodal, with a geometric mean diameter of about 23 nm. The volume size distribution had a geometric volume mean diameter of about 65 nm.

Diesel fuel injection systems are operating at increasingly higher pressure (up to 250 MPa) with smaller clearances, making them more sensitive to diesel fuel contaminants. Most liquid particle counters have difficulty detecting particles <4 μm in diameter and are unable to distinguish between solid and semi-solid materials. The low conductivity of diesel fuel limits the use of the Coulter counter. This raises the need for a new method to characterize small (<4 μm) fuel contaminants. We propose and evaluate an aerosolization method for characterizing solid particulate matter in diesel fuel that can detect particles as small as 0.5 μm. The particle sizing and concentration performance of the method were calibrated and validated by the use of seed particles added to filtered diesel fuel. A size dependent correction method was developed to account for the preferential atomization and subsequent aerosol conditioning processes to obtain the liquid-borne particle concentration.