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The trace contaminant control system (TCCS) located in the International Space Station's (ISS) U.S. laboratory module employs physical adsorption, thermal catalytic oxidation, and chemical adsorption to remove trace chemical contamination produced by equipment offgassing and anthropogenic sources from the cabin atmosphere. The chemical adsorption stage, consisting of a packed bed of granular lithium hydroxide (LiOH), is located after the thermal catalytic oxidation stage and is designed to remove acid gas byproducts that may be formed in the upstream oxidation stage. While in service on board the ISS, the LiOH bed exhibited a change in flow resistance that leading to flow control difficulties in the TCCS. Post flight evaluation revealed LiOH granule size attrition among other changes. An experimental program was employed to investigate mechanisms hypothesized to contribute to the change in the packed bed's flow resistance.

On occasion, seemingly normal operations can have significant effects upon the closed environment of the International Space Station (ISS). An example of such a case occurred on February 20, 2002 when a nominal Metal Oxide (MetOx) canister regeneration operation onboard the ISS resulted in an unexpected, foul odor that affected the crew and station operations. A case study summarizing the root cause for the event and steps taken to ensure that future MetOx regeneration operations proceed safely is presented. Included in the summary are engineering analyses and environmental monitoring results supporting the root cause assessment as well as testing conducted and flight operations changes implemented to ensure safe operations.