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Selective catalytic reduction (SCR) has become the mainstream approach for removing heavy-duty (HD) diesel engine NOx emissions. Highly efficient SCR systems are a key enabling technology allowing engines to be calibrated for very high NOx output with a resultant gain in fuel consumption while still maintaining NOx emissions compliance. One key to the successful implementation of high efficiency SCR at elevated engine out NOx levels is the ability to introduce significantly more AdBlue into the exhaust flow while still ensuring complete ammonia production and avoiding the formation of deposits. This paper presents a body of experimental work conducted on an exhaust test bench using optical techniques including high-speed imaging and phase Doppler interferometry (PDI), applied under representative exhaust conditions to a HD diesel engine after-treatment system with optical access inside the mixer tube. Two different sprays were used to dose AdBlue onto the mixing device.